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Pattern Recognition Methods for Thermal Drift Correction in Atomic Force Microscopy Imaging

机译:原子力显微镜成像中热漂移校正的模式识别方法

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摘要

Atomic Force Microscopy (AFM) is a fundamental tool for the investigation of a wide range of mechanical properties on nanoscale due to the contact interaction between the AFM tip and the sample sur-face. The information recorded with AFM is stored and synthesized by imaging the sample properties to be studied. Distortions and unwanted effects in AFM images can be produced both due to instrumental sources or sample unknown bad responses. The focus of this paper is on an algorithm for distortion corrections for AFM recorded images due to the convolution of thermal drift and unknown polymer compliance. When a sequence of AFM images correspondent to the same polymeric area is acquired, it is common to observe the convolution of thermal drift with surface modifications due to the AFM tip stresses. The surface modifica-tions are material properties and add knowledge to the response of the materials on nanoscale. As a conse-quence, a suitable de-convolution of the thermal drifts on the recorded images needs to be developed. Because soft polymeric samples can present unwanted height alteration due to the stressing AFM tip contact, we present a method that combines a thermal drifts correcting tool (where the original images are modified using a suitable mapping function) with a height rescaling method. In turn, an image matching method based on a Tikhonov functional is developed between topography data and the surface elastic maps, respectively. The precision achieved and the fast computation time required make our methods particularly useful for image analysis on soft polymeric samples as well as in a wide range of other scanning probe microscopy appli-cations.
机译:原子力显微镜(AFM)是研究AFM尖端与样品表面之间接触相互作用的纳米级广泛机械性能的基本工具。通过AFM记录的信息通过对要研究的样品特性进行成像来存储和合成。 AFM图像中的失真和不良影响可能是由于仪器来源或样品未知的不良反应而产生的。本文的重点是由于热漂移和未知聚合物顺应性的卷积而对AFM记录图像进行畸变校正的算法。当获得对应于相同聚合物区域的一系列AFM图像时,通常会观察到由于AFM尖端应力而导致的热漂移与表面改性的卷积。表面改性是材料的特性,为纳米级的材料响应增加了知识。因此,需要对记录的图像上的热漂移进行适当的反卷积。由于柔软的聚合物样品会由于应力性AFM尖端接触而出现不希望的高度变化,因此我们提出了一种结合了热漂移校正工具(使用适当的映射函数修改原始图像)和高度缩放方法的方法。继而,在地形数据和表面弹性图之间分别开发了基于Tikhonov函数的图像匹配方法。所获得的精度和所需的快速计算时间使我们的方法特别适用于对软聚合物样品以及广泛的其他扫描探针显微镜应用进行图像分析。

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