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Preparation and characterization of A1N/FeCoSiB magnetoelectric thin film composites

机译:AlN / FeCoSiB磁电薄膜复合材料的制备与表征

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The preparation process of A1N/FeCoSiB thin film composites has been studied in detail in this work. The results indicate that annealing is more effective to improve the intensity of A1N (002) peak compared with changing sputtering parameters. After annealing at 500℃, the A1N film possesses the highest intensity of (002) peak, typical columnar microstructure and root-mean-square (rms) roughness of 5 nm. The coercivity (H_c) of FeCoSiB film decreases significantly after annealing in magnetic field. After annealing at 350℃, a minimum H_c of 2.6 Oe is obtained in FeCoSiB film, contributing to the achievement of most pronounced magnetic field sensitivity. The magnetoelectric (ME) voltage coefficient α_(ME) up to 101 V/cm Oe is obtained at DC bias magnetic field (H_(dc)) of 10 Oe and at the frequency (f) of 1 kHz. Furthermore, the thin film composites display an AC magnetic field sensitivity of l.enT/√Hz at 1kHz.
机译:本文详细研究了AlN / FeCoSiB薄膜复合材料的制备工艺。结果表明,与改变溅射参数相比,退火更有效地改善了AlN(002)峰的强度。在500℃退火后,AlN薄膜具有最高的(002)峰强度,典型的柱状组织和均方根粗糙度(5nm)。磁场退火后,FeCoSiB薄膜的矫顽力(H_c)大大降低。在350℃退火后,FeCoSiB薄膜的最低H_c为2.6 Oe,有助于实现最显着的磁场灵敏度。在10 Oe的直流偏置磁场(H_(dc))和1 kHz的频率(f)处获得高达101 V / cm Oe的磁电(ME)电压系数α_(ME)。此外,薄膜复合材料在1kHz时的交流磁场灵敏度为l.enT /√Hz。

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