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Facile and scalable synthesis of uniform MgO/Carbon Black nano-admixture for microstructural and mechanical property improvement of magnesia-carbon refractory bricks

机译:方便,可扩展地合成均匀的MgO /炭黑纳米掺合料,以改善镁碳耐火砖的微观结构和力学性能

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摘要

Facile and scalable synthesis method of MgO/Carbon Black nano-admixture as an additive for MgO/C refractory bricks has been developed via simple precipitation method. The main idea of the present work lies on the precipitation of magnesium hydroxide in well dispersed/stabilized carbon black nanoparticle suspension resulting in Mg(OH)(2)/CB nano-admixture preparation. Furthermore, applying such colloidal suspension of CBs prevent the sever agglomeration of Mg-containing precipitate and make simple precipitation method as a reliable synthesis method of nano-structured MgO. Finally, different analytical methods including X-ray diffractometer, Scanning electron microscopy, Cold crushing strength and physical properties measurement have been utilized to study the effect of such nano-admixture on the microstructural and mechanical properties of typical MgO/C refractory bricks. (C) 2016 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
机译:通过简单的沉淀法,已经开发了一种简便,可扩展的MgO /炭黑纳米掺合料作为MgO / C耐火砖添加剂的合成方法。本工作的主要思想在于,氢氧化镁在充分分散/稳定的炭黑纳米颗粒悬浮液中的沉淀,从而制备Mg(OH)(2)/ CB纳米混合物。此外,使用这种CBs的胶体悬浮液可防止含Mg的沉淀物严重团聚,并使简单的沉淀方法成为可靠的纳米MgO合成方法。最后,利用不同的分析方法,包括X射线衍射仪,扫描电子显微镜,冷压强度和物理性能测量,研究了这种纳米掺合料对典型MgO / C耐火砖的微观结构和力学性能的影响。 (C)2016 Elsevier Ltd和Techna Group S.r.l.版权所有。

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