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Physicochemical Characterization and the Comparison of Chitin and Chitin Modified with Maleic Anhydride

机译:甲壳素和马来酸酐改性的甲壳素的理化性质与比较

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摘要

Firstly, chitin was modified via ring-opening reaction with maieic anhydride in lithium chloride/ N,N-dimethylacetamide. Then, both chitin and chitin modified with maleic anhydride (CMA) were characterized by Fourier transform infrared (FTIR) spectroscopy, X-ray diffraction (XRD) method, uitraviolet-visible (UV-Vis) spectroscopy, and scanning electron microscopy (SEM). Thermogravimetric analysis (TGA) was performed to investigate the thermal stability of chitin and CMA. TGA results showed that chitin is thermally more stable than CMA. In addition, the electrical conductivity of chitin and CMA was also measured. Electrical conductivity measurement results showed that the electrical conductivity of CMA (4.3x1 10~(-4) S cm~(-1)) is more than that of chitin (6.5 x 10~(-6) S cm~(-1)).
机译:首先,在氯化锂/ N,N-二甲基乙酰胺中,与甲酸酐经开环反应改性甲壳质。然后,通过傅立叶变换红外(FTIR)光谱,X射线衍射(XRD)方法,紫外可见(UV-Vis)光谱和扫描电子显微镜(SEM)对几丁质和经马来酸酐(CMA)改性的几丁质进行表征。 。进行热重分析(TGA)以研究甲壳质和CMA的热稳定性。 TGA结果表明,几丁质比CMA具有更高的热稳定性。另外,还测量了几丁质和CMA的电导率。电导率测量结果表明,CMA(4.3x1 10〜(-4)S cm〜(-1)的电导率高于几丁质(6.5 x 10〜(-6)S cm〜(-1)的电导率。 )。

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