C-Phosphorylation of Unsaturated Ketones with Phosphorus Pentachloride

Larina L. I.; Komarova T. N.; Rozinov V. G.

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C-Phosphorylation of Unsaturated Ketones with Phosphorus Pentachloride

机译：五氯化磷将不饱和酮进行C-磷酸化

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C-Phosphorylation of a number of unsaturated ketones with phosphorus pentachloride has been studied. Structure of the obtained dienyltrichlorophosphonium hexachlorophosphorates was established by means of H-1, C-13, and P-31 NMR spectroscopy.

机译：已经研究了五氯化磷对许多不饱和酮的C-磷酸化作用。借助H-1，C-13和P-31 NMR光谱确定所获得的六氯磷酸二烯基三氯phosph的结构。

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《Russian Journal of General Chemistry》 |2016年第3期|共3页
作者
Larina L. I.; Komarova T. N.; Rozinov V. G.;
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正文语种 eng
中图分类化学;
关键词
phosphorus pentachloride; phosphorus-containing dienes; unsaturated ketones; hexachlorophosphorates; NMR spectroscopy;

机译：五氯化磷;含磷的二烯;不饱和酮;六氯代磷酸酯;NMR光谱;

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专利

1. C-Phosphorylation of Unsaturated Ketones with Phosphorus Pentachloride [J] . Larina L. I., Komarova T. N., Rozinov V. G. Russian Journal of General Chemistry . 2016,第3期

机译：五氯化磷将不饱和酮进行C-磷酸化
2. New synthesis and cyclopropanation of alpha-phenylselanyl alpha,beta-unsaturated ketones with non-stabilized phosphorus ylides [J] . Redon S, Leleu S, Pannecoucke X, Tetrahedron . 2008,第39期

机译：α-苯基杂戊基α，β-不饱和酮与不稳定的磷化氢的新合成和环丙烷化
3. Synthesis and characterization of photosensitive phosphorus based polymers containing alpha,beta-unsaturated ketones in the main chain [J] . Kaniappan K, Murugavel S Journal of Macromolecular Science. Pure and Applied Chemistry . 2005,第12期

机译：主链含α，β-不饱和酮的光敏磷基聚合物的合成与表征
4. ESI-MS Studies on the Self-Assembly of Valine into Oligo-Peptides Mediated by Phosphorus Pentachloride [C] . Journal of Tsinghua University: science and technology . 2001

机译：ESI-MS研究缬氨酸自组装成五氯化磷介导的寡肽
5. I. Studies on the competitive thermal fragmentation of beta-hydroxyketones: Dehydration vs. formaldehyde elimination. II. Studies on the conjugate addition of Grignard reagents to alpha,beta-unsaturated ketones: Isolation and oxidation of E and Z enols of a ketone. [D] . Logaraj, Sundaram. 1988

机译：I.β-羟基酮竞争性热裂解的研究：脱水与甲醛消除。二。格氏试剂到α，β-不饱和酮上的共轭加成研究：酮的E和Z烯醇的分离和氧化。
6. Phosphorus Pentachloride Promoted gem-Dichlorination of 2′- and 3′-Deoxynucleosides [O] . Fabio da Paixao Soares, Elisabetta Groaz, Piet Herdewijn 2018

机译：五氯化磷促进2-和3-脱氧核苷的宝石二氯化
7. Evidence for a Chlorocarbenium Ion in Reactions of alpha-Ethynyl Ketones with Phosphorus Pentachloride. [O] . Naser-Ud-Din, Lars Skattebøl, Jens Jørgen Led, 1983

机译：用磷五氯化磷α-乙炔基酮反应的氯氟鎓离子的证据。

C-Phosphorylation of Unsaturated Ketones with Phosphorus Pentachloride

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