First optically active P-alkoxy derivative of pa Undated phosphacymantrene: synthesis, structure, and chiroptical properties

A. F. Smolyakov; A. G. Ginzburg; V. V. Bashilov

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First optically active P-alkoxy derivative of pa Undated phosphacymantrene: synthesis, structure, and chiroptical properties

机译：pa的首个旋光活性P-烷氧基衍生物未取代的磷酸环丙三烯：合成，结构和手性

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The solvopalladation reaction of 2,5-diphenylphosphacymantrene with Na2PdCl4, AcONa, and optically active carbinol (S)-(—)-2-methylbutanol was carried out. Optically active complex 3 was obtained and characterized by X-ray diffraction analysis and circular dichroism (CD), ~(13)C and ~(31)P NMR, IR, and UV spectra.

机译：进行了2，5-二苯基磷酰基扁桃烯与Na 2 PdCl 4，AcONa和旋光性甲醇（S）-（-）-2-甲基丁醇的溶剂醇溶反应。获得光学活性配合物3，并通过X射线衍射分析和圆二色性（CD），〜（13）C和〜（31）P NMR，IR和UV光谱表征。

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《Russian Chemical Bulletin》 |2013年第4期|共6页
作者
A. F. Smolyakov; A. G. Ginzburg; V. V. Bashilov;
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正文语种 eng
中图分类化学;
关键词
phosphacymantrene; alkoxypalladation; optical activity; UV; NMR; and CD spectra; X-ray diffraction analysis.;

机译：磷酰基man烯;烷氧基钯;光学活性;紫外光谱;NMR;CD光谱;X射线衍射分析。;

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1. First optically active P-alkoxy derivative of pa Undated phosphacymantrene: synthesis, structure, and chiroptical properties [J] . A. F. Smolyakov, A. G. Ginzburg, V. V. Bashilov Russian Chemical Bulletin . 2013,第4期

机译：pa的首个旋光活性P-烷氧基衍生物未取代的磷酸环丙三烯：合成，结构和手性
2. Optically active fluoro-substituted polyaniline prepared in organic media: The synthesis, chiroptical properties, and comparison with optically active non-substituted polyaniline [J] . Hino T, Kumakura T, Kuramoto N Polymer: The International Journal for the Science and Technology of Polymers . 2006,第15期

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First optically active P-alkoxy derivative of pa Undated phosphacymantrene: synthesis, structure, and chiroptical properties

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