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Synthesis, characterization and catalytic application of Au NPs-reduced graphene oxide composites material: an eco-friendly approach

机译:Au NPs还原氧化石墨烯复合材料的合成,表征和催化应用:一种生态友好的方法

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In this paper, we have reported the synthesis of Au NPs-reduced graphene oxide (rGO) composites under microwave irradiation using ascorbic acid as eco-friendly reducing agent. The formation of Au NPs-rGO composites was confirmed by UV/Visible spectroscopy, DRIFT spectroscopy, TGA, XRD analysis, SAXS and HRTEM. HRTEM analysis results show that the particle size of the Au NPs formed on rGO nanosheets were in the range of 2-20 nm which is also supported by SAXS analysis results. The synthesized Au NPs-rGO composites were successfully utilized for the aerobic oxidation of benzyl alcohols to their corresponding aldehydes.
机译:在本文中,我们报道了在微波辐射下使用抗坏血酸作为生态友好型还原剂合成Au NPs还原的氧化石墨烯(rGO)复合材料的方法。紫外/可见光谱,DRIFT光谱,TGA,XRD分析,SAXS和HRTEM证实了Au NPs-rGO复合材料的形成。 HRTEM分析结果表明,rGO纳米片上形成的Au NP的粒径在2-20 nm范围内,这也得到了SAXS分析结果的支持。合成的金纳米颗粒-rGO复合材料已成功地用于苯甲醇的好氧氧化为其相应的醛。

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