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Chemical and morphological features of nanofilled composite resin: Influence of finishing and polishing procedures and fluoride solutions

机译:纳米填充复合树脂的化学和形态特征:精加工和抛光程序以及氟化物溶液的影响

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摘要

This study evaluated the influence of finishing and polishing procedures and different fluoride solutions on superficial morphology and chemistry of the nanofilled composite resin Supreme XT (3M) through the EDX analysis and SEM evaluation. Circular specimens (n = 30) of 10 mm diameter and 2 mm thickness were prepared, with half of the sample assays finished and polished with Super-Snap? sandpaper. The experimental groups were divided according to the presence or absence of finishing and polishing and solutions (artificial saliva, 0.05% of manipulated sodium fluoride solution, Fluordent Reach, Oral B, Fluorgard). Specimens were immersed in each respective solution for 1 min per day, during 60 days and stored in artificial saliva at 37 ± 1°C between immersion periods. Topography and chemical analysis was qualitative. It was observed that specimens submitted to finishing and polishing procedures had lower superficial degradation. Fluoride solutions promoted superficial alterations on specimens, being the highest degradation obtained with Fluordent Reach. It can be concluded that finishing and polishing procedures and the immersion media influence the superficial morphology of composite resin tested; the Fluordent Reach was the fluoride solution that most affected the material's surface.
机译:这项研究通过EDX分析和SEM评估,评估了抛光和抛光程序以及不同的氟化物溶液对纳米填充复合树脂Supreme XT(3M)的表面形态和化学性质的影响。准备了直径为10毫米,厚度为2毫米的圆形样品(n = 30),其中一半样品分析完成并用Super-Snap?抛光。砂纸。根据是否进行精加工和抛光以及溶液(人工唾液,0.05%的氟化钠溶液,Fluordent Reach,口服B,Fluorgard)将实验组划分。将标本每天在每种溶液中浸泡60分钟,每天1分钟,在两次浸泡之间的37±1°C的人工唾液中保存。形貌和化学分析是定性的。观察到,经过精加工和抛光的样品表面降解较低。氟化物溶液促进了标本的表面变化,这是使用Fluordent Reach获得的最高降解。可以得出结论,精加工和抛光程序以及浸入介质会影响所测试的复合树脂的表面形态。氟化物达到率是最影响材料表面的氟化物溶液。

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