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Fabrication of miniature parts using nano-sized powders and an environmentally friendly binder through micro powder injection molding

机译:通过微粉末注射成型,使用纳米级粉末和环保粘合剂制造微型零件

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摘要

Component miniaturization is increasingly gaining importance in numerous microsystem technologies, including medical technology, biotechnology, and drive technology. In this study, two types of nano-sized powder, namely, metal (stainless steel 316L) and ceramic (yttria-stabilized zirconia), were used to fabricate miniature parts through micro powder injection molding. Micro parts were produced by mixing powders with a binder system, followed by injection, debinding, and sintering process. Partially water-soluble binder system with surfactant addition was used to mix with either stainless steel 316L or yttria-stabilized zirconia nanopowder to form feedstock to avoid the agglomeration of fine powder and environmentally hazardous organic binder. The polyethylene glycol loss in water was observed after a rapid removal period in the first 60 min of immersion for the micro parts. Approximately 99 % of the polymethyl methacrylate binder was removed after pyrolysis at 450 A degrees C for 2.5 h. Sintered ceramic and metallic parts showed a relative density that is approximately 97 % of theoretical density and free of defects. Hardness of approximately 221 and 1,200 Hv was achieved for the fabricated micro parts using stainless steel 316L and yttria-stabilized zirconia powders, respectively.
机译:组件的小型化在包括医疗技术,生物技术和驱动技术在内的众多微系统技术中越来越重要。在这项研究中,使用两种类型的纳米级粉末,即金属(316L不锈钢)和陶瓷(氧化钇稳定的氧化锆),通过微粉末注射成型来制造微型零件。通过将粉末与粘合剂体系混合,然后进行注射,脱脂和烧结工艺来生产微型零件。使用添加了表面活性剂的部分水溶性粘合剂体系与316L不锈钢或氧化钇稳定的氧化锆纳米粉混合以形成原料,以避免细粉和对环境有害的有机粘合剂结块。在浸泡的最初60分钟内,对微型零件进行了快速去除之后,观察到水中的聚乙二醇损失。在450 A的温度下热解2.5小时后,除去了约99%的聚甲基丙烯酸甲酯粘合剂。烧结的陶瓷和金属零件的相对密度约为理论密度的97%,并且没有缺陷。分别使用316L不锈钢和氧化钇稳定的氧化锆粉末制成的微型零件,其硬度分别约为221和1200 Hv。

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