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首页> 外文期刊>Metallurgical and Materials Transactions, A. Physical Metallurgy and Materials Science >The Evolution of Annealing Textures in 90 Pct Drawn Copper Wire
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The Evolution of Annealing Textures in 90 Pct Drawn Copper Wire

机译:90 Pct拉制铜线退火织构的演变

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An electrolytic copper rod was drawn in 24 passes to a 90 pct reduction in area and subsequently annealed under various conditions. The global texture of the drawn wire, as measured by X-ray methods, showed a fiber texture approximated by a strong <111> and a weak <100> component. However, its microtexture, as measured by electron backscattered diffraction (EBSD), indicated that the major <111> + minor <100> duplex fiber texture was dominant only in the center region, while a relatively diffuse texture developed with a somewhat higher density of orientations having a <11w>// wire axis in the middle and surface regions. The inhomogeneous texture in the as-deformed wire gave rise to an inhomogeneous microstructure and texture after annealing. When annealed at 300 deg C or 600 deg C for 3 hours, the wire developed a duplex fiber texture consisting of major <100> + minor <111> components in the center region, a strong <100> fiber texture in the middle region, and a weak texture consisting of <111> and <100> components with the <111> component being slightly stronger in the surface region. When the drawn wire was annealed at the high temperature of 700 deg C, the texture at short annealing times was similar to that of the wire annealed at the lower temperatures of 300 deg C and 600 deg C for 3 hours, but prolonged annealing gave rise to a texture ranging from the <111> to <112> components due to abnormal grain-growth that started in the surface region. The recrystallization texture consisting of the major <100> + minor <111> components was explained by the strain-energy-release maximization (SERM) model, in which the recrystallization texture is determined such that the absolute maximum principal stress direction due to dislocations in the deformed state is along the minimum elastic-modulus direction in recrystallized grains. On the other hand, the abnormal grain-growth texture was attributed to grain-boundary mobility differences between differently oriented grain.
机译:在24道次拉伸中拉出电解铜棒,以减少90%的面积,然后在各种条件下进行退火。通过X射线方法测得的拉丝的整体纹理显示出纤维质地,其强<111>成分和<100>弱成分近似。但是,通过电子反向散射衍射(EBSD)测得的微织构表明,主要的<111> +次要的<100>双工纤维织构仅在中心区域占主导地位,而相对分散的织构则具有更高的密度。在中部和表面区域的导线轴方向为<11w> //的方向。变形后的金属丝的不均匀织构导致退火后的微观结构和织构不均匀。当在300℃或600℃退火3小时时,焊丝会形成双纤维组织,其中心区域主要由<100> +次要的<111>成分组成,中部区域则具有较强的<100>纤维组织,以及由<111>和<100>成分组成的较弱的质地,其中<111>成分在表面区域中稍强。当将拉制的线材在700℃的高温下退火时,短退火时间的织构类似于在300℃和600℃的较低温度下退火3小时的线材的织构,但是延长退火会产生由于在表面区域开始出现异常的晶粒长大,所以其纹理范围从<111>到<112>。用应变能释放最大化(SERM)模型解释了由主要的<100> +次要的<111>成分组成的再结晶织构,在该模型中,确定了再结晶织构,使得由于位错引起的绝对最大主应力方向在再结晶晶粒中,变形状态沿着最小弹性模量方向。另一方面,异常晶粒生长织构归因于不同取向晶粒之间的晶界迁移率差异。

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