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Extracting electron backscattering coefficients from backscattered electron micrographs

机译:从反向散射电子显微照片中提取电子反向散射系数

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摘要

Electron backscattering micrographs possess the so-called Z-contrast, carrying information about the chemical compositions of phases present in microstructures. The intensity at a particular point in the backscattered electron micrograph is proportional to the signal detected at a corresponding point in the scan raster, which is, in turn, proportional to the electron backscattering coefficient of a phase at that point. This article introduces a simple method for extracting the electron backscattering coefficients of phases present in the microstructure, from the backscattered electron micrographs. This method is able to convert the micrograph's greyscale to the backscattering-coefficient-scale. The prerequisite involves the known backscattering coefficients for two phases in the micrograph. In this way, backscattering coefficients of other phases can be determined. The method is unable to determine the chemical compositions of phases or the presence of an element only from analysing the backscattered electron micrograph. Nevertheless, this method was found to be very powerful when combined with energy dispersive spectroscopy, and the calculations of backscattering coefficients.
机译:电子反向散射显微照片具有所谓的Z对比度,可携带有关微观结构中相化学组成的信息。反向散射电子显微照片中特定点的强度与在扫描光栅的相应点处检测到的信号成正比,而强度又与该点处相的电子反向散射系数成正比。本文介绍了一种简单的方法,用于从反向散射电子显微照片中提取微观结构中存在的相的电子反向散射系数。这种方法能够将显微照片的灰度转换为反向散射系数比例。前提条件涉及显微照片中两相的已知反向散射系数。这样,可以确定其他相位的后向散射系数。该方法仅通过分析反向散射电子显微照片不能确定相的化学组成或元素的存在。但是,与能量色散光谱和反向散射系数的计算相结合时,发现该方法非常有效。

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