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Microstructure and mechanical behavior of direct metal laser sintered Inconel alloy 718

机译:直接金属激光烧结Inconel 718合金的组织和力学性能

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In this paper, we investigate microstructure and quasi-static mechanical behavior of the direct metal laser sintered Inconel 718 superalloy as a function of build direction (BD). The printed material was further processed by annealing and double-aging, hot isostatic pressing (HIP), and machining. We characterize porosity fraction and distribution using micro X-ray computed tomography (mu XCT), grain structure and crystallographic texture using electron backscattered diffraction (EBSD), and mechanical response in quasi-static tension and compression using standard mechanical testing at room temperature. Analysis of the mu XCT imaging shows that majority of porosity develops in the outer layer of the printed material. However, porosity inside the material is also present. The EBSD measurements reveal formation of columnar grains, which favor < 001 > fiber texture components along the BD. These measurements also show evidence of coarse-grained microstructure present in the samples treated by HIP. Finally, analysis of grain boundaries reveal that HIP results in a large number of annealing twins compared to that in samples that underwent annealing and double-aging. The yield strength varies with the testing direction by approximately 7%, which is governed by a combination of grain morphology and crystallographic texture. In particular, we determine tension-compression asymmetry in the yield stress as well as anisotropy of the material flow during compression. We find that HIP lowers yield stress but improves ductility relative to the annealed and aged material. These results are discussed and critically compared with the data reported for wrought material in the same condition. (C) 2016 Elsevier Inc. All rights reserved.
机译:在本文中,我们研究了直接金属激光烧结Inconel 718高温合金作为组织方向(BD)的函数的微观结构和准静态力学行为。通过退火和双时效,热等静压(HIP)和机加工对印刷材料进行进一步处理。我们使用微X射线计算机断层扫描(mu XCT),使用电子背散射衍射(EBSD)的晶粒结构和晶体织构以及准静态拉伸和压缩的机械响应(在室温下使用标准机械测试)来表征孔隙率和分布。对mu XCT成像的分析表明,大部分孔隙形成在印刷材料的外层。但是,材料内部也存在孔隙。 EBSD测量揭示了圆柱状晶粒的形成,这有利于沿BD的<001>纤维纹理成分。这些测量结果还显示了在通过HIP处理的样品中存在粗晶粒微观结构的证据。最后,对晶界的分析表明,与经过退火和双时效处理的样品相比,HIP可以产生大量的退火孪晶。屈服强度随测试方向变化约7%,这取决于晶粒形态和晶体学织构的组合。特别是,我们确定屈服应力中的拉伸-压缩不对称以及压缩过程中材料流动的各向异性。我们发现,相对于退火和时效的材料,HIP降低了屈服应力,但改善了延展性。对这些结果进行了讨论,并与相同条件下锻造材料的报告数据进行了严格比较。 (C)2016 Elsevier Inc.保留所有权利。

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