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Looking for a surface treatment to deposit a reactive element with potential industrial use in high temperature oxidation field

机译:寻找一种表面处理方法来沉积反应性元素,在高温氧化领域具有潜在的工业用途

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摘要

In order to introduce a so-called reactive element simultaneously at all the surfaces of a NiCr (Ni-20wt.%Cr-1.5wt.%Si) metallic substrate alloy, an easy to apply surface treatment was used: an yttrium containing thin film (constituted of a hydrated yttrium hydroxide nitrate) was electrodeposited from a mixed water-ethanol solution. After a thermal conversion treatment at 600℃ under argon, leading to an Y{sub}2O{sub}3 coating, specimens were submitted to high-temperature oxidation testing, under artificial air at atmospheric pressure, in order to evaluate in these conditions the effect of the coatings on the behaviour of the studied alloy. Expected effects of the introduced reactive element (REE) were effectively shown: decrease of the coated sample weight gain, suppression of the formation of the base metal oxides and change of the oxide grains morphology.
机译:为了在NiCr(Ni-20wt。%Cr-1.5wt。%Si)金属基体合金的所有表面上同时引入所谓的反应元素,使用了易于应用的表面处理:含钇薄膜(由水合氢氧化钇硝酸盐构成)(由水-乙醇混合溶液)电沉积。在氩气下于600℃进行热转化处理后,生成Y {sub} 2O {sub} 3涂层,然后在大气压的人造空气下对样品进行高温氧化测试,以便在这些条件下评估涂层对所研究合金性能的影响。有效显示了引入的反应性元素(REE)的预期效果:涂层样品重量增加的减少,贱金属氧化物形成的抑制和氧化物晶粒形态的变化。

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