Solvothermal synthesis, crystal structure, and characterization of an oxothiomolybdate, [N(CH3)(4)](4)Mo6O6S14 exhibiting a new Mo6O6S14 core

Ellermeier J.; Bensch W.; Nather C.

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Solvothermal synthesis, crystal structure, and characterization of an oxothiomolybdate, [N(CH3)(4)](4)Mo6O6S14 exhibiting a new Mo6O6S14 core

机译：溶剂热合成，晶体结构和表征的氧代硫代钼酸盐[N（CH3）（4）]（4）Mo6O6S14展示了一个新的Mo6O6S14核心

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Reaction of elemental sulfur, sodiummolybdate dihydrate and tetramethylammonium hydroxide under solvothremal conditions leads to the new oxothiomolybdate: [N(CH3)(4)](4)Mo6O6S14. The structure consists of three Mo2O2S4-units which art: connected by two mu(3)-S atoms. The compound is characterized by single-crystal methods and vibrational spectra. [References: 26]

机译：元素硫条件下元素硫，钼酸钠二水合物和氢氧化四甲基铵的反应生成新的氧代硫代钼酸盐：[N（CH3）（4）]（4）Mo6O6S14。该结构由三个Mo2O2S4单元组成，该单元具有：通过两个mu（3）-S原子连接。该化合物的特征在于单晶方法和振动光谱。 [参考：26]

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《Inorganic Chemistry: A Research Journal that Includes Bioinorganic, Catalytic, Organometallic, Solid-State, and Synthetic Chemistry and Reaction Dynamics》 |1999年第20期|共4页
作者
Ellermeier J.; Bensch W.; Nather C.;
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正文语种 eng
中图分类化学;
关键词
Functional-group; Thio-complexes; Molybdenum; Reactivity; Tungsten; lt; mo3s13gt; 2; Anions;

机译：官能团;硫杂配合物;钼;反应性;钨;mo3s13 2;阴离子;

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1. Solvothermal synthesis, crystal structure, and characterization of an oxothiomolybdate, [N(CH3)(4)](4)Mo6O6S14 exhibiting a new Mo6O6S14 core [J] . Ellermeier J., Bensch W., Nather C. Inorganic Chemistry: A Research Journal that Includes Bioinorganic, Catalytic, Organometallic, Solid-State, and Synthetic Chemistry and Reaction Dynamics . 1999,第20期

机译：溶剂热合成，晶体结构和表征的氧代硫代钼酸盐[N（CH3）（4）]（4）Mo6O6S14展示了一个新的Mo6O6S14核心
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8. Metal Atom Synthesis of Metallaboron Clusters. 8. Synthesis of New Cobalt, Iron, and Nickel Clusters Derived from 2,6-C2B7H11. Structural Characterization of 2-ETA 6-C6(CH3)3H3 Fe-1,6-C2B7H9, 6-ETA 6-C6(CH3)3H3 Fe-9,10-C2B7H11, and 5,7,8-(CH3)-11,7,8,10- ETA 3-C4(CH3)4H niC3B7H7. [R] . Sneddon, L. G., Briguglio, J. J. 1986

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Solvothermal synthesis, crystal structure, and characterization of an oxothiomolybdate, [N(CH3)(4)](4)Mo6O6S14 exhibiting a new Mo6O6S14 core

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