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Characterization of mechanisms of hot deformation of as-cast nickel aluminide alloy

机译:铸铝镍合金热变形机理的表征

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The hot deformation behavior of as-cast Ni_3AI alloy has been characterized on the basis of its flow stress variation obtained by isothermal constant true strain rate compression testing in the temperature range 1100-1250deg C and strain rate range 0.001-10 s~(-1). The mechanisms of hot working have been evaluated using four generations of materials modeling techniques, which included shape of stress-strain curves, kinetic analysis, processing maps and dynamical systems approach. The material exhibited a steady-state flow behavior at slower strain rates but flow softening associated sometimes with broad oscillations, was observed at higher strain rates. The flow stress data did not obey the kinetic rate equation over the entire regime of testing but a good fit has been obtained in the intermediate range of temperatures (1150-l200deg C). In this range, a stress exponent value of 6.5 and an apparent activation energy of about 750 kJ/mol have been evaluated. Microstructural investigations have shown that the matrix 7' phase undergoes dynamic recovery in the presence of harder 7 colonies The processing maps revealed four different domains out of which three are interpreted to represent cracking processes. The fourth domain, which has a peak efficiency of about 44 percent, occurred at 1250deg C/0.00l s~(-1). Microstructural observations revealed that this domain represents dynamic recrystallization (DRX) of 7 phase and is desirable for hot working the material. The material exhibits flow instabilities when deformed in the intermediate temperature regime at strain rates higher than 1 s~(-1). and these are manifested as shear localization.
机译:根据铸态Ni_3Al合金的热变形行为,通过在1100-1250℃温度范围和0.001-10 s〜(-1)等温常数真应变速率压缩试验中获得的流变应力来表征。 )。已经使用四代材料建模技术评估了热加工的机理,其中包括应力-应变曲线的形状,动力学分析,加工图和动力学系统方法。该材料在较低的应变速率下表现出稳态的流动行为,但在较高的应变速率下观察到有时与宽振动相关的流动软化。在整个测试范围内,流动应力数据均未遵循动力学速率方程,但在中间温度范围(1150至1200摄氏度)下获得了很好的拟合度。在此范围内,已评估出应力指数值为6.5和表观活化能约为750 kJ / mol。微观结构研究表明,在较硬的7个菌落的存在下,基质7'相经历了动态恢复。加工图显示了四个不同的域,其中三个域被解释为代表裂解过程。第四域的峰值效率约为44%,出现在1250℃/ 0.00l s〜(-1)。微观结构观察表明,该域代表7相的动态重结晶(DRX),对于热加工材料是理想的。当材料在中等温度范围内以高于1 s〜(-1)的应变速率变形时,其流动不稳定。这些表现为剪切局部化。

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