Synthesis and spectral[IR,~1H,~(13)C,and ~(11)B] properties of 2-(N-arylsalicylaldimino)-4,4,5,5-tetramethyl-1,3,2-dioxaborolanes

Sunita Goyal; Anirudh Singh

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Synthesis and spectral[IR,~1H,~(13)C,and ~(11)B] properties of 2-(N-arylsalicylaldimino)-4,4,5,5-tetramethyl-1,3,2-dioxaborolanes

机译：2-（N-芳基水杨基醛二氨基）-4,4,5,5-四甲基-1,3,2-二氧杂硼烷的合成及光谱[IR，〜1H，〜（13）C，〜（11）B]性质

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Reactions in 1:1 molar ratio of 2-isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane with N-arylsali-cylaldimines (LH=HOC_6 H_4CH=NC6H5,HOC_6H_4CH=NC_6H_4Me2-2,6,HOC_6H_4CH=NC6H_2Me3-2,4,6,HOC6H4CH=NC6H3Et2-2,6,and HOC6H4CH=NC6H3-r~i2-2,6 in benzene afford new cyclic compounds of boron containing pinacolate and salicylaldiminate groups.These new derivatives have been characterized by elemental analysis and spectroscopic [IR,NMR (~1H,~(13)C,and ~(11)] studies as well as by molecular weight determinations.

机译：以1：1摩尔比反应的2-异丙氧基-4,4,5,5-四甲基-1,3,2-二氧杂硼烷与N-芳基水杨基-亚乙基亚胺（LH = HOC_6 H_4CH = NC6H5，HOC_6H_4CH = NC_6H_4Me2-2,6苯中的HOC_6H_4CH = NC6H_2Me3-2,4,6，HOC6H4CH = NC6H3Et2-2,6和HOC6H4CH = NC6H3-r〜i2-2,6提供了新的含频哪酸酯和水杨基二酰亚胺基团的硼环化合物。通过元素分析和光谱[IR，NMR（〜1H，〜（13）C，〜（11）]]研究以及通过分子量测定进行表征。

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《Indian Journal of Chemistry, Section A. Inorganic, Physical, Theoretical & Analytical》 |2001年第6期|共4页
作者
Sunita Goyal; Anirudh Singh;
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中图分类化学;化学工业;
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机译：4,4,5,5-四甲基-2- [1,3,6,8-四溴-7-（4,4,5,5-四甲基-1,3,2-二氧杂硼烷-2-基）py- 2-基] -1,3,2-二氧杂硼烷

Synthesis and spectral[IR,~1H,~(13)C,and ~(11)B] properties of 2-(N-arylsalicylaldimino)-4,4,5,5-tetramethyl-1,3,2-dioxaborolanes

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