A convenient synthesis of 4,8,9-trimethoxybenz[f]indenone, a potential BCD ring intermediate for stealthins and kinamycins

Dipakranjan Mal; Sujit Ghorai; Nirmal Hazra

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A convenient synthesis of 4,8,9-trimethoxybenz[f]indenone, a potential BCD ring intermediate for stealthins and kinamycins

机译：方便合成4,8,9-三甲氧基苯并[f]茚满酮，这是一种潜在的BCD环隐身蛋白和kinamycins中间体

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摘要

A convenient regiospecific synthesis of 4, 8, 9-trimethoxy-benz[f] indenone 6 has been developed which involves Hauser reaction between phthalide sulfone 3 and enone 4, followed by O-methylation of 5a and retro Diels-Alder reaction of 5b.

机译：已开发出方便的区域特异性合成4、8、9-三甲氧基-苯并[f]茚满酮6的方法，该方法涉及邻苯二甲砜3和烯酮4之间的豪瑟反应，接着进行5a的O-甲基化和5b的逆狄尔斯-阿尔德反应。

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《Indian Journal of Chemistry, Section B. Organic Including Medicinal》 |2001年第10期|共3页
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Dipakranjan Mal; Sujit Ghorai; Nirmal Hazra;
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中图分类化学;化学工业;
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1. A convenient synthesis of 4,8,9-trimethoxybenz[f]indenone, a potential BCD ring intermediate for stealthins and kinamycins [J] . Dipakranjan Mal, Sujit Ghorai, Nirmal Hazra Indian Journal of Chemistry, Section B. Organic Including Medicinal . 2001,第10期

机译：方便合成4,8,9-三甲氧基苯并[f]茚满酮，这是一种潜在的BCD环隐身蛋白和kinamycins中间体
2. Kinamycin biosynthesis. Synthesis, isolation, and incorporation of stealthin C. An aminobenzo[b]fluorene [J] . Steven J.Gould, Chris R.Martha C.Cone, Jiong Chen The Journal of Organic Chemistry . 1997,第2期

机译：动霉素的生物合成。隐身蛋白C的合成，分离和结合。氨基苯并[b]芴
3. Synthetic studies of kinamycin antibiotics: Stereoselective synthesis of the highly oxygenated D-ring and construction of the ABD-ring system of kinamycins [J] . Ouzouni M.-D., Fokas D. European journal of organic chemistry . 2013,第27期

机译：卡那霉素抗生素的合成研究：高氧D环的立体选择性合成和卡那霉素ABD环系统的构建
4. 36-disubstituted cyclohex-2-en-1-ones as intermediates for synthesis of liquid crystals with lateral substituted cyclohexane or benzene rings [C] . Vladimir Bezborodov, Institute of Applied Physical Problems, Minsk, Liquid Crystals: Materials Science and Applications . 1995

机译：36-二取代的环己-2-烯-1-酮作为中间体合成侧向取代的环己烷或苯环的液晶
5. Part I. Extending allenyl azide cycloaddition chemistry: Photochemistry and copper(i) mediation. Part II. Efforts toward the total synthesis of (-)-kinamycin F. Part III. Effect of strength and symmetry of hydrogen bonds on quinone reduction potential [D] . Hester, David Keith, II 2008

机译：第一部分：扩展烯丙基叠氮化物环加成化学：光化学和铜（i）介导。第二部分（-）-卡那霉素F的全合成方面的努力。氢键的强度和对称性对醌还原电位的影响
6. Studies on polynuclear furoquinones. Part 1: Synthesis of tri- and tetra-cyclic furoquinones simulating BCD/ABCD ring system of furoquinone diterpenoids [O] . Faruk Hasan Shaik, Gandhi Kumar Kar 2009

机译：多核呋喃醌的研究。第1部分：模拟呋喃醌二萜的BCD / ABCD环系统的三环和四环呋喃醌的合成
7. A Biogenetically-Inspired Synthesis of a Ring-D Model of Kinamycin F: Insights into the Conformation of Ring D [O] . -1

机译：一种生物地灵感合成Kinamycin F的Ring-D模型F：洞穴洞穴的洞察
8. Surface Science Investigation of Potential Intermediates, Catalysts, and Promoters in the Synthesis of Higher Alcohols by Metals: Progress Report [R] . Barteau, M. A. 1987

机译：金属合成高级醇中潜在中间体，催化剂和促进剂的表面科学研究：进展报告

A convenient synthesis of 4,8,9-trimethoxybenz[f]indenone, a potential BCD ring intermediate for stealthins and kinamycins

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