Synthesis and Bowl-in-Bowl Assembly of a Geodesic Phenylene Bowl

Ikemoto Koki; Kobayashi Ryo; Sato Sota; Isobe Hiroyuki

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Synthesis and Bowl-in-Bowl Assembly of a Geodesic Phenylene Bowl

机译：测地亚苯基碗的合成和碗碗组装

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摘要

A phenylene multiring with a corannulenoidal skeleton was synthesized. Geodesic constraints over 20 phenylene panels resulted in its nanometer-sized, bowl-shaped molecular structure, which was unequivocally revealed by crystallographic analysis. The crystal structure also showed the presence of a bowl-in-bowl dimeric assembly, which was driven by entropic factors in solution.

机译：合成了具有Corannulenoid骨架的亚苯基多次。在20个亚苯基板上产生的测地约束导致其纳米尺寸的碗状分子结构，其通过晶体分析毫不含糊地透露。晶体结构还显示出碗内二聚体组件的存在，其被溶液中的熵因子驱动。

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来源
《Angewandte Chemie》 |2017年第23期|共4页
作者
Ikemoto Koki; Kobayashi Ryo; Sato Sota; Isobe Hiroyuki;
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作者单位

Univ Tokyo Dept Chem JST ERATO Isobe Degenerate Integrat Project Bunkyo Ku Hongo 7-3-1 Tokyo 1130033 Japan;

Tohoku Univ Adv Inst Mat Res Aoba Ku Sendai Miyagi 9808577 Japan;

Univ Tokyo Dept Chem JST ERATO Isobe Degenerate Integrat Project Bunkyo Ku Hongo 7-3-1 Tokyo 1130033 Japan;

Univ Tokyo Dept Chem JST ERATO Isobe Degenerate Integrat Project Bunkyo Ku Hongo 7-3-1 Tokyo 1130033 Japan;

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原文格式 PDF
正文语种 eng
中图分类应用化学;
关键词
macrocycles; meta-phenylene; molecular recognition; nanostructures; self-assembly;

机译：宏ycles;meta-亚苯基;分子识别;纳米结构;自我组装;

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专利

1. Synthesis and Bowl-in-Bowl Assembly of a Geodesic Phenylene Bowl [J] . Ikemoto Koki, Kobayashi Ryo, Sato Sota, Angewandte Chemie . 2017,第23期

机译：测地亚苯基碗的合成和碗碗组装
2. Assembly of new Schiff base ligands derived from vitamin B6 and stabilization through complexation of N,N '-bis-(pyridoxylideneimine)-o-phenylene: Synthesis and X-ray Structural features of pyridoxal/o-phenylenediamine adducts and of [UO2(H2pyr2phen)Cl]NO3 and [UO2(Hpyr2phen)Cl] {pyr2phen=N,Nprime-bis-(pyridoxylideneiminato)2-phenylene} [J] . Back DF, de Oliveira GM, Lang ES, Polyhedron: The International Journal for Inorganic and Organometallic Chemistry . 2008,第12期

机译：源自维生素B6的新席夫碱配体的组装和通过N，N'-双-（吡啶氧基亚胺）-邻苯撑的络合作用的稳定作用：吡pyr醛/邻苯二胺加合物和[UO2（H2pyr2phen））Cl] NO3和[UO2（Hpyr2phen）Cl] {pyr2phen = N，Nprime-bis-（-pyridoxylideneiminato）2-phenylene}
3. Big macrocyclic assemblies of carboranes (big MACs): synthesis and crystal structure of a macrocyclic assembly of four carboranes containing alternate ortho- and meta-carborane icosahedra linked by para-phenylene units [J] . Fox MA., Howard JAK., MacBride JAH., Journal of Organometallic Chemistry . 2003,第1a2期

机译：碳硼烷的大环组装体（大MAC）：四个碳硼烷的大环组装体的合成和晶体结构，其中包含通过对亚苯基单元连接的交替的邻位和间位碳烷二十面体
4. Synthesis and Molecular Recognition of Nanometer-sized Geodesic Phenylene Bowl [C] . Koki Ikemoto, Ryo Kobayashi, Sota Sato 日本化学会春季年会講演予稿集 . 2018

机译：纳米大小测地亚苯甲烯的合成与分子识别
5. Synthesis of oligo(p-phenylene vinylene)s and functionalization of silicon(100) and/or silicon(111) surfaces with oligo(p-phenylene vinylene)s. [D] . Sun, Chivin. 2009

机译：寡（对亚苯基亚乙烯基）的合成和用寡（对亚苯基亚乙烯基）的硅（100）和/或硅（111）表面的官能化。
6. Synthesis and Photophysical and ElectroluminescentProperties of Poly(14-phenylene–ethynylene)-alt-poly(14-phenylene–vinylene)s with Various Dissymmetric Substitutionof Alkoxy Side Chains [O] . Nassima Bouguerra, Aleš Růžička, Christoph Ulbricht, -1

机译：合成及光物理和电致发光各种不对称取代的聚（14-亚苯基-亚乙炔基）-alt-聚（14-亚苯基-亚乙烯基）的性质烷氧基侧链
7. Synthesis and Bowl‐in‐Bowl Assembly of a Geodesic Phenylene Bowl [O] . Koki Ikemoto, Ryo Kobayashi, Sota Sato, 2017

机译：测地亚苯基碗的合成和碗碗组装
8. Synthesis and Characterization of Poly(Oxy(2-Methyl-1,3-Phenylene)-Oxyisophthaloyl-b-(2-Methyl-1,3- Phenylene)Oxyterephthaloyl)Oxy. [R] . Polk, M. B., Onwumere, F. C. 1984

机译：聚（氧（2-甲基-1,3-亚苯基） - 氧代间苯二酰基-b-（2-甲基-1,3-亚苯基）氧对苯二甲酰基）氧基的合成和表征。

Synthesis and Bowl-in-Bowl Assembly of a Geodesic Phenylene Bowl

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