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Fabrication and characterization of a mullite-foamed ceramic reinforced by in-situ SiC whiskers

机译:原位SIC晶须加固莫来石发泡陶瓷的制造与表征

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In this study, a new mullite-foamed ceramic, reinforced with in-situ SiC whiskers (MCS) and applied as the insulating lining of thermal equipment used in cement production, was investigated. Compared with a conventional mullite-foamed ceramic (MC), the MCS phase composition, microstructure, compressive strength, thermal conductivity and alkali corrosion resistance were investigated by using X-ray diffraction, scanning electron microscopy, energy dispersive X-ray spectroscopy, and Factsage (R) software. The results showed that after being fired in granular coke, the SiC whiskers formed into MCS struts and were distributed in the pores between the interconnected needle-like mullite. Although the formation of SiC with higher conduction slightly increased MCS thermal conductivity, it significantly enhanced the compressive strength and alkali corrosion resistance of the foamed ceramic. Compared with the MC, although the MCS had higher bulk density (3.9%), and higher thermal conductivity (9.5% at 800 degrees C), it was more important that greatly improved compressive strength (by 60%) and better alkali corrosion resistance was achieved.
机译:在本研究中,研究了一种新的莫来石泡沫陶瓷,用原位SiC晶须(MCS)加强并作为水泥生产中使用的热设备的绝缘衬里应用。与传统的莫来石发泡陶瓷(MC)相比,通过使用X射线衍射,扫描电子显微镜,能量分散X射线光谱和Factsage来研究MCS相组合物,微观结构,抗压强度,导热性和碱腐蚀性(r)软件。结果表明,在粒状焦炭中烧制后,形成MCS支柱的SiC晶须并分布在互连的针状莫来石之间的孔中。尽管形成具有更高传导的SiC略微增加MCS导热率,但显着提高了发泡陶瓷的抗压强度和碱腐蚀性。与MC相比,虽然MCS具有更高的堆积密度(3.9%),导热性较高(800℃下为9.5%),但大大提高的抗压强度(乘60%)和更好的碱腐蚀性是更重要的实现。

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