Preparation of a stoichiometric molecularly imprinted polymer for auramine O and application in solid‐phase extraction

Pataer Parezhati; Muhammad Turghun; Turahun Yunusjan; Yang Wenwu; Aihebaier Sailemayi; Wubulikasimu Muyasier; Chen Lingxin

摘要

Abstract >We describe a stoichiometric approach to the synthesis of molecularly imprinted polymers specific for auramine O. Using the stoichiometric interaction in molecular imprinting, no excess of binding sites is necessary and binding sites are only located inside the imprinted cavities. The free base of the template was obtained to facilitate the interaction with the monomers. Itaconic acid was selected as the functional monomer, and stoichiometric ratio of the interaction with the free base was investigated. The molecularly imprinted polymer preparation conditions such as cross‐linker, molar ratio, porogen were optimized as divinylbenzene, 1:2:20 and chloroform/N,N‐dimethylformamide, respectively. Under the optimum conditions, a good imprinting effect and very high selectivity were achieved. A solid‐phase extraction method was developed using the molecularly imprinted polymers as a sorbent and extraction procedure was optimized. The solid‐phase extraction method showed a high extraction recovery for auramine O in its hydrochloride form and free form compared to its analogues. The results strongly indicated that stoichiometric imprinting is an efficient method for development of high selectivity molecularly imprinted polymers for auramine O. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</标题> >我们描述了一种化学计量的方法，用于合成用于金刚胺O.的分子印迹聚合物。使用在分子印迹中的化学计量相互作用，不需要过量的结合位点，并且结合位点仅位于印迹腔内。获得模板的游离碱以促进与单体的相互作用。选择衣康酸作为官能单体，研究了与游离碱的相互作用的化学计量比。分子印迹的聚合物制备条件如交联剂，摩尔比，孔胶，分别优化为二乙烯基苯，1：2：20和氯仿/ N，N-二甲基甲酰胺。在最佳条件下，实现了良好的印记效果和非常高的选择性。使用分子印迹聚合物开发固相提取方法，因为优化了吸附剂和提取方法。与其类似物相比，固相萃取方法对其盐酸盐形式的高萃取恢复和其盐酸盐形式和游离形式。结果强烈表明，化学计量印记是一种高可选择的氨胺印迹聚合物的高选择性的高选择性方法。</ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35800/'>《Journal of separation science.》</a> <b style="margin: 0 2px;">|</b><span>2019年第8期</span><b style="margin: 0 2px;">|</b><span>共10页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Pataer Parezhati&option=202" target="_blank" rel="nofollow">Pataer Parezhati;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Muhammad Turghun&option=202" target="_blank" rel="nofollow">Muhammad Turghun;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Turahun Yunusjan&option=202" target="_blank" rel="nofollow">Turahun Yunusjan;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yang Wenwu&option=202" target="_blank" rel="nofollow">Yang Wenwu;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Aihebaier Sailemayi&option=202" target="_blank" rel="nofollow">Aihebaier Sailemayi;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wubulikasimu Muyasier&option=202" target="_blank" rel="nofollow">Wubulikasimu Muyasier;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Chen Lingxin&option=202" target="_blank" rel="nofollow">Chen Lingxin;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Key Laboratory of Oil and Gas Fine Chemicals Ministry of Education &</p> <p>Xinjiang Uygur Autonomous Region College of Chemistry and Chemical EngineeringXinjiang UniversityUrumqi P. R. China;</p> <p>Key Laboratory of Oil and Gas Fine Chemicals Ministry of Education &</p> <p>Xinjiang Uygur Autonomous Region College of Chemistry and Chemical EngineeringXinjiang UniversityUrumqi P. R. China;</p> <p>Key Laboratory of Oil and Gas Fine Chemicals Ministry of Education &</p> <p>Xinjiang Uygur Autonomous Region College of Chemistry and Chemical EngineeringXinjiang UniversityUrumqi P. R. China;</p> <p>Key Laboratory of Oil and Gas Fine Chemicals Ministry of Education &</p> <p>Xinjiang Uygur Autonomous Region College of Chemistry and Chemical EngineeringXinjiang UniversityUrumqi P. R. China;</p> <p>Key Laboratory of Oil and Gas Fine Chemicals Ministry of Education &</p> <p>Xinjiang Uygur Autonomous Region College of Chemistry and Chemical EngineeringXinjiang UniversityUrumqi P. R. China;</p> <p>Key Laboratory of Oil and Gas Fine Chemicals Ministry of Education &</p> <p>Xinjiang Uygur Autonomous Region College of Chemistry and Chemical EngineeringXinjiang UniversityUrumqi P. R. China;</p> <p>CAS Key Laboratory of Coastal Environment Processes and Ecological Remediation Yantai Institute of Coastal Zone ResearchChinese Academy of SciencesYantai P. R. China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/159.html" title="化学">化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=auramine O hydrochloride&option=203" rel="nofollow">auramine O hydrochloride;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=molecularly imprinted polymers&option=203" rel="nofollow">molecularly imprinted polymers;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=rational design&option=203" rel="nofollow">rational design;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=solid‐phase extraction&option=203" rel="nofollow">solid‐phase extraction;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=stoichiometric interactions&option=203" rel="nofollow">stoichiometric interactions;</a> </p> <div class="translation"> 机译：盐酸氨酸o;分子印迹聚合物;合理设计;固相提取;化学计量相互作用; 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