Performance comparison of dispersive solid‐phase extraction and multiplug filtration cleanup methods for the determination of tefuryltrione in plant and environmental samples using UHPLC–MS/MS

Yu Yang; Tao Yan; Dong Fengshou; Xu Jun; Liu Xingang; Wu Xiaohu; Ji Mingshan; Zheng Yongquan

摘要

Abstract > The detection frequencies of tefuryltrione, a new type of 4‐hydroxyphenyl‐pyruvate dioxygenase inhibitor herbicide, are rarely reported, probably because of the paucity of analytical methods. Herein, an effective and sensitive analytical method has been developed to detect tefuryltrione in vegetables (tomato and cucumber), cereals (rice and corn), soil, and water by ultra high performance liquid chromatography coupled with tandem mass spectrometry. Comparisons of the performances of dispersive solid‐phase extraction and multiplug filtration cleanup methods were carried out for tefuryltrione in complex matrices. Extraction solvents and purification sorbents were further optimized for dispersive solid‐phase extraction. Tefuryltrione was analyzed with electrospray ionization in the positive mode within 2.0?min. Mean recoveries for tefuryltrione were 75.4–108.9% with relative standard deviations less than 11.0% at three fortification levels (10, 100, 500?μg/kg) in the sample matrixes. Limits of quantification ranged from 0.70 to 5.12?μg/kg, and an excellent linearity ( R 2 ≥ 0.9902) was obtained for tefuryltrione at concentrations of 5–1000?μg/L. The results showed that the developed dispersive solid‐phase extraction method could serve as an effective, sensitive, and robust method for routine monitoring of tefuryltrione residue in plants and environmental samples. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><abstract type =“main”xml：lang =“en”> <title type =“main”>抽象</ title> > Tefuryltrione的检测频率，一种新型的4-羟基苯基 - 丙酮酸二氧化酶抑制剂除草剂，很少报道，可能是因为分析方法的缺乏。在此，已经开发了一种有效和敏感的分析方法，以通过超高效液相色谱法与串联质谱耦合，以检测蔬菜（番茄和黄瓜），谷物（稻米和玉米），谷物（水稻和玉米），土壤和水中的Tefuryltrione。在复合基质中对Tefuryltrione进行分散固相提取和倍增过滤清除方法的比较。进一步优化提取溶剂和纯化吸附剂，用于分散固相萃取。用电喷雾电离在2.0≤min的阳性模式下分析Tefuryltrione。 Tefuryltrione的平均回收率为75.4-108.9％，在样品基质中的三种固化水平（10,100,500Ωμg/ kg）中的相对标准偏差小于11.0％。定量限制范围为0.70至5.12？μg/ kg，并且在浓度为5-1000Ω·μg/ L.结果表明，发育的色散固相提取方法可用作植物和环境样品常规监测Tefuryltrione残基的有效，敏感和稳健的方法。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35800/'>《Journal of separation science.》</a> <b style="margin: 0 2px;">|</b><span>2017年第22期</span><b style="margin: 0 2px;">|</b><span>共11页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yu Yang&option=202" target="_blank" rel="nofollow">Yu Yang;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Tao Yan&option=202" target="_blank" rel="nofollow">Tao Yan;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Dong Fengshou&option=202" target="_blank" rel="nofollow">Dong Fengshou;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Xu Jun&option=202" target="_blank" rel="nofollow">Xu Jun;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Liu Xingang&option=202" target="_blank" rel="nofollow">Liu Xingang;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wu Xiaohu&option=202" target="_blank" rel="nofollow">Wu Xiaohu;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ji Mingshan&option=202" target="_blank" rel="nofollow">Ji Mingshan;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zheng Yongquan&option=202" target="_blank" rel="nofollow">Zheng Yongquan;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>College of Plant ProtectionShenyang Agricultural UniversityShenyang People's Republic of China;</p> <p>State Key Laboratory for Biology of Plant Diseases and Insect PestsInstitute of Plant Protection Chinese Academy of Agricultural SciencesBeijing People's Republic of China;</p> <p>State Key Laboratory for Biology of Plant Diseases and Insect PestsInstitute of Plant Protection Chinese Academy of Agricultural SciencesBeijing People's Republic of China;</p> <p>State Key Laboratory for Biology of Plant Diseases and Insect PestsInstitute of Plant Protection Chinese Academy of Agricultural SciencesBeijing People's Republic of China;</p> <p>State Key Laboratory for Biology of Plant Diseases and Insect PestsInstitute of Plant Protection Chinese Academy of Agricultural SciencesBeijing People's Republic of China;</p> <p>State Key Laboratory for Biology of Plant Diseases and Insect PestsInstitute of Plant Protection Chinese Academy of Agricultural SciencesBeijing People's Republic of China;</p> <p>College of Plant ProtectionShenyang Agricultural UniversityShenyang People's Republic of China;</p> <p>State Key Laboratory for Biology of Plant Diseases and Insect PestsInstitute of Plant Protection Chinese Academy of Agricultural SciencesBeijing People's Republic of China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/159.html" title="化学">化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=herbicides&option=203" rel="nofollow">herbicides;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=sample treatment&option=203" rel="nofollow">sample treatment;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=tandem mass spectrometry&option=203" rel="nofollow">tandem mass spectrometry;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=tefuryltrione&option=203" rel="nofollow">tefuryltrione;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=ultra high performance liquid chromatography&option=203" rel="nofollow">ultra high performance liquid chromatography;</a> </p> <div class="translation"> 机译：除草剂;样品处理;串联质谱;Tefuryltrione;超高效液相色谱法; </div> </li> </ul> </div> </div> <div class="literature cardcommon" id="literaturereference" style="display:none"> <div class="similarity "> <h3 class="all_title" id="enpatent111">引文网络</h3> <div class="referencetab clearfix"> <ul id="referencedaohang"> <li dataid="referenceul">参考文献</li> <li dataid="citationul">引证文献</li> <li dataid="commonreferenceul">共引文献</li> <li dataid="commoncitationul">同被引文献</li> <li dataid="tworeferenceul">二级参考文献</li> <li dataid="twocitationul">二级引证文献</li> </ul> </div> <div class="reference_details" id="referenceList"> <ul id="referenceul"></ul> <ul id="citationul"></ul> <ul id="commonreferenceul"></ul> <ul id="commoncitationul"></ul> <ul id="tworeferenceul"></ul> <ul id="twocitationul"></ul> </div> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704025846367.html">Performance comparison of dispersive solid‐phase extraction and multiplug filtration cleanup methods for the 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