Rapid and noninvasive quality control of anhydrous milk fat by PTR‐MS: The effect of storage time and packaging

Pedrotti M.; Khomenko I.; Cappellin L.; Fontana M.; Somenzi M.; Falchero L.; Arveda M.; Fogliano V.; Biasioli F.

摘要

Abstract >In this study, proton transfer reaction‐mass spectrometry (PTR‐MS), coupled with a time‐of‐flight mass analyzer and a multipurpose automatic sampler, was evaluated as a rapid and nondestructive tool for the quality control of anhydrous milk fat. Anhydrous milk fats packed in cardboard and bag‐in‐box were compared during refrigerated shelf life at 4°C for 9?months. Anhydrous milk fat samples were taken at 120, 180, and 240?days and measured by PTR‐MS during storage at 50°C for 11?days. Univariate and multivariate data analysis were performed in order to classify samples according to the packaging type and compare aromatic profiles. >Markers related to both packaging and storage duration were identified, and all stored samples were clearly distinguishable from reference fresh samples. Significant differences in some key butter aroma compounds such as 2‐pentanone, 2‐heptanone, 2/3‐methylbutanal, acetoin, and butanoic acid were observed between different types of packaging. During the refrigerated storage, differences related to packaging are more evident, while during the storage at 50°C, the fat oxidation induced by the high temperature becomes the most relevant phenomenon independently of the packaging type. These results indicate the importance of avoiding anhydrous milk fat storage at 50°C for long times during industrial production processes. All together data demonstrated the viability of PTR‐MS as a rapid and high‐sensitivity tool in agroindustry quality control program. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><abstract xmlns =“http://www.wiley.com/namespaces/wiley”type =“main”xml：lang =“en”> <title type =“main”>抽象</ title> >研究质子转移反应 - 质谱（PTR-MS）与飞行时间分析仪和多用途自动采样器相结合，被评估为无水乳脂肪的质量控制的快速和无损工具。在4°C的冷藏保质期间将无水奶脂肪包装在纸板和箱内箱内箱内箱内袋装9？在120,180和240℃下拍摄无水乳脂肪样品，并在储存期间在50℃下通过PTR-MS测量11？天。进行单变量和多变量数据分析，以便根据包装类型对样品进行分类，并比较芳族型材。鉴定出与包装和储存持续时间相关的标记，并且所有存储的样品都清晰可区分。样品。在不同类型的包装之间观察到某些关键黄油芳香化合物如2-戊酮，2-庚酮，2 / 3-甲基丁醛，丙酮素和丁酸的显着差异。在冷藏储存期间，与包装相关的差异更明显，而在储存期间在50℃下，由高温引起的脂肪氧化成为独立于包装类型的最相关的现象。这些结果表明在工业生产过程中避免在50℃下在50℃下避免无水乳脂储存的重要性。所有一起数据都证明了PTR-MS作为Agroindustry质量控制程序中的快速和高灵敏度工具的可行性。</ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" > 著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-34906/'>《Journal of mass spectrometry: JMS 》</a> <b style="margin: 0 2px;">|</b><span>2018年第9期</span><b style="margin: 0 2px;">|</b> <span>共10页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Pedrotti M.&option=202" target="_blank" rel="nofollow">Pedrotti M.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Khomenko I.&option=202" target="_blank" rel="nofollow">Khomenko I.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Cappellin L.&option=202" target="_blank" rel="nofollow">Cappellin L.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Fontana M.&option=202" target="_blank" rel="nofollow">Fontana M.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Somenzi M.&option=202" target="_blank" rel="nofollow">Somenzi M.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Falchero L.&option=202" target="_blank" rel="nofollow">Falchero L.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Arveda M.&option=202" target="_blank" rel="nofollow">Arveda M.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Fogliano V.&option=202" target="_blank" rel="nofollow">Fogliano V.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Biasioli F.&option=202" target="_blank" rel="nofollow">Biasioli F.;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Research and Innovation Center Department of Food Quality and NutritionFondazione Edmund MachVia E. Mach 1 San Michele all'Adige TN 38010 Italy;</p> <p>Research and Innovation Center Department of Food Quality and NutritionFondazione Edmund MachVia E. Mach 1 San Michele all'Adige TN 38010 Italy;</p> <p>Research and Innovation Center Department of Food Quality and NutritionFondazione Edmund MachVia E. Mach 1 San Michele all'Adige TN 38010 Italy;</p> <p>Soremartec Italia srlPiazzale Ferrero 1 Alba Cuneo 12051 Italy;</p> <p>Soremartec Italia srlPiazzale Ferrero 1 Alba Cuneo 12051 Italy;</p> <p>Soremartec Italia srlPiazzale Ferrero 1 Alba Cuneo 12051 Italy;</p> <p>Soremartec Italia srlPiazzale Ferrero 1 Alba Cuneo 12051 Italy;</p> <p>Food Quality &</p> <p>Design GroupWageningen University &</p> <p>ResearchWageningen WG NL‐6708 Netherlands;</p> <p>Research and Innovation Center Department of Food Quality and NutritionFondazione Edmund MachVia E. Mach 1 San Michele all'Adige TN 38010 Italy;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li> <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span> <a href="https://www.zhangqiaokeyan.com/clc/1187.html" title="分析化学">分析化学 ;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=anhydrous milk fat&option=203" rel="nofollow">anhydrous milk fat;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=industrial quality control&option=203" rel="nofollow">industrial quality control;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=packaging&option=203" rel="nofollow">packaging;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=PTR‐MS&option=203" rel="nofollow">PTR‐MS;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=shelf life&option=203" rel="nofollow">shelf life;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=VOCs&option=203" rel="nofollow">VOCs;</a> </p> <div class="translation"> 机译：无水牛奶脂肪;工业质量控制;包装;PTR-MS;保质期;VOCS; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" 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href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=徐楠&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 徐楠</a> <span> <a href="/journal-cn-6610/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 黑龙江医药科学 </a> </span> <span> . 2003</span><span> ,第001期</span> </span> </div> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/academic-journal-cn_practical-journal-aesthetic-plastic-surgery_thesis/0201267451412.html">非侵入性脂肪雕塑机治疗肥胖症临床报告</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=曹志明&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 曹志明</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=方哲鑫&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,方哲鑫</a> <span> <a href="/journal-cn-51416/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 实用美容整形外科杂志 </a> </span> <span> . 1999</span><span> ,第003期</span> </span> </div> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-19272_thesis/020222181854.html">牛奶塑料包装膜性能及其质量控制方法探讨</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=康小红&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 康小红</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=胡新宇&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,胡新宇</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=刘卫星&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,刘卫星</a> <span> <a href="/conference-cn-19272/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 中国奶业协会2008年年会 </a> <span> <span> . 2008</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/02031369053.html">非药物干预缓解侵入性护理操作所致新生儿疼痛效果的系统评价</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=王松&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 王松</a> <span> . 2011</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06120103709952.html">非酒精性脂肪性肝病、非酒精性脂肪性肝炎和/或肝纤维化的非侵入性诊断</a> <b>[P]</b> . <span> 中国专利： CN111065748A </span> <span> . 2020-04-24</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120103968735.html">非酒精性脂肪性肝病、非酒精性脂肪性肝炎和/或肝纤维化的非侵入性诊断</a> <b>[P]</b> . <span> 中国专利： CN111032884A </span> <span> . 2020-04-17</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130401327029.html">process of obtaining fully hydrogenated anhydrous milk fat, fully hydrogenated anhydrous milk fat thus obtained and using it</a> <b>[P]</b> . <span> 外国专利：  BR102019000428A2 </span> <span> . 2020-07-28</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：获得完全氢化的无水乳脂的方法，由此获得的完全氢化的无水乳脂并使用它 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130442365500.html">METHOD FOR PREPARING OF A PURIFIED ANHYDROUS CONCEMETHOD FOR PREPARING OF A PURIFIED ANHYDROUS CONCENTRATE OF MILK FAT AND A DEVICE FOR REALIZING THERNTRATE OF MILK FAT AND A DEVICE FOR REALIZING THEREOF EOF</a> <b>[P]</b> . <span> 外国专利：  UA70544A </span> <span> . 2004-10-15</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：制备纯净无水浓缩乳脂的方法，制备纯净无水浓缩乳脂的方法以及实现纯净脂肪的装置及其实现该方法的设备 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130409362805.html">METHODS FOR SELECTIVE AND SENSITIVE MILK FAT QUANTITATION AND MILK QUALITY CONTROL USING BODIPY BASED MILK FAT FLUORESCENT SENSORS</a> <b>[P]</b> . <span> 外国专利：  IN201617044414A </span> <span> . 2017-04-14</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：使用基于身体的乳脂荧光传感器进行选择性和敏感乳脂定量和乳汁质量控制的方法 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" style="bottom: 19px;z-index: 999;" onclick="ywcd('0704025633030','4',7,2,1,'',this,24)" class="delivery" prompt="010401" title="通过人工服务将文献原文发送至邮箱" >获取原文</div> <div class="journalsub-pop-up" style="display: none"> <div class="journal-sub"> <h2>期刊订阅</h2> <img 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