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Thermally stable and high impact toughness chopped PI fiber-reinforced PEEK composites

机译:热稳态和高冲击韧性切碎的PI纤维增强PEEK复合材料

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摘要

Chopped polyimide (PI) fiber-reinforced polyether ether ketone (PEEK) composites with different fiber content (0%, 10%, 20%, and 30%) were prepared via melt extrusion using a twin-screw extruder. The impact strength of these composites significantly improved from 4.9 kJ m-2 to 9.3 kJ m-2 with the increase of the PI fiber content from 0% to 30%. Tensile strength, tensile modulus, and flexural strength also increased with the increase in PI fiber content. In addition, the heat deflection temperature increased significantly from 160 degrees C to 318 degrees C. The results of the dynamic mechanical analysis revealed that the storage modulus increased considerably. The relationship between mold temperature and composite properties was investigated, and using differential scanning calorimetry, it was shown that the increase in mold temperature improved the degree of polymer crystallization and the bonding capability of the fiber and resin interface. As a result, the mechanical properties of the composite material were improved.
机译:使用双螺杆挤出机通过熔融挤出制备具有不同纤维含量(0%,10%,20%和30%)的纤维含量(PEE)的聚酰亚胺(PI)纤维增强聚醚醚酮(PEEK)复合材料。这些复合材料的冲击强度从4.9kJ m-2至9.3kJ m-2显着改善,随着0%至30%的Pi纤维含量增加。随着Pi纤维含量的增加,拉伸强度,拉伸模量和抗弯强度也增加。此外,热偏转温度从160℃升高到318℃。动态机械分析的结果显示储存模量显着增加。研究了模塑温度和复合性能之间的关系,并使用差示扫描量热法,示出了模具温度的增加改善了聚合物结晶程度和纤维和树脂界面的粘合能力。结果,改善了复合材料的机械性能。

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