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Optical and Structural Properties of Indium Sulfide Thin Film Produced by CBD Method

机译:CBD法生产的硫化物薄膜的光学和结构性能

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Indium sulfide thin films were prepared by chemical bath deposition (CBD) method on a glass substrate at a sedimentation time of about 45 min. The films were grown at different bath temperature as 30, 55, 70 and 85 degrees C. The crystallinity, nanostructures and morphology of the prepared films have been investigated by using X-ray diffraction (XRD), scanning electron microscopy (SEM) and atomic force microscopy (AFM) analyses. Optical reflectance of layers was measured in the energy range of 1.5-5.5 eV by spectrophotometer instrument. Kramers-Kronig relations were used to calculate the optical constants. The X-ray diffraction spectrum showed that by increasing in growth temperature, crystalline structure was changed. According to the atomic force microscope images, with increasing growth temperature, roughness increases consistently. Optical results revealed that the highest optical band gap of 3.4 eV and the highest transmittance of 90% were achieved at higher deposition temperature (85 degrees C).
机译:通过化学浴沉积(CBD)方法在玻璃基板上在约45分钟的沉降时间上制备硫化物薄膜。将膜在不同的浴温中生长为30,55,70和85℃。通过使用X射线衍射(XRD),扫描电子显微镜(SEM)和原子已经研究了制备薄膜的结晶度,纳米结构和形态。力显微镜(AFM)分析。通过分光光度计仪器在1.5-5.5 eV的能量范围内测量层的光学反射率。 Kramers-Kronig关系用于计算光学常数。 X射线衍射光谱表明,通过增加生长温度,改变结晶结构。根据原子力显微镜图像,随着增长温度的增加,粗糙度一致增加。光学结果显示,在较高沉积温度(85℃)下,实现了3.4eV的最高光带隙和90%的最高透射率。

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