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首页> 外文期刊>Propellants, Explosives, Pyrotechnics >Solubilities of 2,6‐Diamino‐3,5‐dinitropyrazine‐1‐oxide in the Binary Mixtures of DMSO+H2O, DMF+H2O and NMP+H2O in the Temperature Range from 293.15?to 323.15?K under the Atmospheric Pressure
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Solubilities of 2,6‐Diamino‐3,5‐dinitropyrazine‐1‐oxide in the Binary Mixtures of DMSO+H2O, DMF+H2O and NMP+H2O in the Temperature Range from 293.15?to 323.15?K under the Atmospheric Pressure

机译：2,6-二氨基-3,5-二硝基吡嗪-1-氧化物在DMSO + H 2 O，DMF + H 2 O，NMP + H 2 O的二元混合物中的溶解度在温度范围内的温度范围内的温度范围内的温度范围内的〜323.15μm

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Abstract > Recrystallization is usually required for the application of 2,6‐Diamino‐3,5‐dinitropyrazine‐1‐oxide (LLM‐105) as an energy material due to its poor crystal morphology. The study of its solubilities in binary solvent mixtures can provide primary support for optimizing the recrystallization and spheroidization conditions of LLM‐105. In the current work, the solubilities of LLM‐105 in the binary mixtures of dimethyl sulfoxide (DMSO)+H <sub>2</sub> O, N,N‐dimethyl‐formamide (DMF)+H <sub>2</sub> O and 1‐methyl‐2‐pyrrolidone (NMP) +H <sub>2</sub> O were measured by the gravimetric method in the temperature range from 293.15?K to 323.15?K under the atmospheric pressure. The results suggest that the solubility of LLM‐105 increases with the increase of temperature and the concentration of the solvent. The experimental data were then fitted with the modified Apelbalt equation, (CNIBS)/Redlich‐Kister equation and Jouyban‐Acree equation. All models fit the experimental data well, indicating that they can be used to predict the solubilities of LLM‐105 in the binary solvent mixtures. The thermodynamic parameters of the dissolution including enthalpy, standard entropy and Gibbs energy were calculated from the experimental data. It was found that the dissolutions of LLM‐105 in all test solvents were endothermic. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 由于其晶体形态差，通常需要2,6-二氨基-3,5-二硝基吡吡嗪-1-氧化物（LLM-105）作为能量材料所需的重结晶。其在二元溶剂混合物中的溶解度的研究可以提供初级载体，用于优化LLM-105的再结晶和球化条件。在当前的工作中，LLM-105在二甲基亚砜（DMSO）+ H的二元混合物中的溶解度 <sub> 2 </ sub> O，N，N-二甲基 - 甲酰胺（DMF）+ H. <sub> 2 </ sub> O和1-甲基-2-吡咯烷酮（NMP）+ H. <sub> 2 </ sub> 通过在大气压下通过293.15·k至323.15 k至323.15μk的温度范围测量o。结果表明，随着温度和溶剂浓度的增加，LLM-105的溶解度增加。然后将实验数据配有改进的apelbalt方程，（CNIB）/ redlich-Kister方程和Jouyban-Acree方程。所有型号均符合实验数据，表明它们可用于预测LLM-105在二元溶剂混合物中的溶解度。从实验数据计算包括焓，标准熵和吉布斯能量的溶解的热力学参数。发现所有测试溶剂中LLM-105的溶解是吸热的。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-29946/'>《Propellants, Explosives, Pyrotechnics》</a> <b style="margin: 0 2px;">|</b><span>2020年第3期</span><b style="margin: 0 2px;">|</b><span>共6页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wang Yuqiao&option=202" target="_blank" rel="nofollow">Wang Yuqiao;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Jin Shaohua&option=202" target="_blank" rel="nofollow">Jin Shaohua;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li Tujuan&option=202" target="_blank" rel="nofollow">Li Tujuan;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Lan Guanchao&option=202" target="_blank" rel="nofollow">Lan Guanchao;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhang Xiaopeng&option=202" target="_blank" rel="nofollow">Zhang Xiaopeng;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhang Zhengzheng&option=202" target="_blank" rel="nofollow">Zhang Zhengzheng;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhou Chang&option=202" target="_blank" rel="nofollow">Zhou Chang;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Chen Yu&option=202" target="_blank" rel="nofollow">Chen Yu;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>School of Materials Science &</p> <p>EngineeringBeijing Institute of TechnologyBeijing 100081 P. R. China;</p> <p>School of Materials Science &</p> <p>EngineeringBeijing Institute of TechnologyBeijing 100081 P. R. China;</p> <p>School of Materials Science &</p> <p>EngineeringBeijing Institute of TechnologyBeijing 100081 P. R. China;</p> <p>School of Materials Science &</p> <p>EngineeringBeijing Institute of TechnologyBeijing 100081 P. R. China;</p> <p>School of Materials Science &</p> <p>EngineeringBeijing Institute of TechnologyBeijing 100081 P. R. China;</p> <p>Research Institute of Gansu Yinguang Chemical Industry GroupBaiyin 730900 P. R. China;</p> <p>China Fortune PressBeijing 100070 P. R. China;</p> <p>School of Materials Science &</p> <p>EngineeringBeijing Institute of TechnologyBeijing 100081 P. R. China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1837.html" title="爆炸物工业、火柴工业">爆炸物工业、火柴工业;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=2&option=203" rel="nofollow">2;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=6-diamino-3&option=203" rel="nofollow">6-diamino-3;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=5-dinitropyrazine-1-oxide&option=203" rel="nofollow">5-dinitropyrazine-1-oxide;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Solubility&option=203" rel="nofollow">Solubility;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Gravimetric method&option=203" rel="nofollow">Gravimetric method;</a> </p> <div class="translation"> 机译：2;6-二氨基-3;5-二硝基吡嗪-1-氧化物;溶解度;重量法; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704024626227.html">Solubilities of 2,6‐Diamino‐3,5‐dinitropyrazine‐1‐oxide in the Binary Mixtures of DMSO+H2O, DMF+H2O and NMP+H2O in the Temperature Range from 293.15?to 323.15?K under the Atmospheric Pressure</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wang Yuqiao&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Wang Yuqiao,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Jin Shaohua&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Jin Shaohua,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li Tujuan&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Li Tujuan,</a> <a href="/journal-foreign-29946/" target="_blank" rel="nofollow" class="tuijian_authcolor">Propellants, Explosives, Pyrotechnics .</a> <span>2020</span><span>,第3期</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：2,6-二氨基-3,5-二硝基吡嗪-1-氧化物在DMSO + H 2 O，DMF + H 2 O，NMP + H 2 O的二元混合物中的溶解度在温度范围内的温度范围内的温度范围内的温度范围内的〜323.15μm</span> </p> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704024626614.html">Erratum: Measurement, Correlation and Thermodynamics of Solubility of 2,6‐Diamino‐3,5‐Dinitropyrazine‐1‐Oxide (LLM‐105) in Eight Solvents</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Bu Rupeng&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Bu Rupeng,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhou Xiaoqing&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Zhou Xiaoqing,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Huang Qi&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Huang Qi,</a> <a href="/journal-foreign-29946/" target="_blank" rel="nofollow" class="tuijian_authcolor">Propellants, Explosives, Pyrotechnics .</a> <span>2018</span><span>,第9期</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：错误：8次溶剂中2,6-二氨基-3,5-二硝基吡吡吡吡吡吡嗪-1-氧化物（LLM-105）的溶解度的测量，相关性和热力学</span> </p> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704024626442.html">Measurement, Correlation and Thermodynamics of Solubility of 2,6-Diamino-3,5-Dinitropyrazine-1-Oxide (LLM-105) in Eight Solvents</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Bu Rupeng&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Bu Rupeng,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhou Xiaoqing&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Zhou Xiaoqing,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Huang Qi&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Huang Qi,</a> <a href="/journal-foreign-29946/" target="_blank" rel="nofollow" class="tuijian_authcolor">Propellants, Explosives, Pyrotechnics .</a> <span>2017</span><span>,第12期</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：2,6-二氨基-3,5-二硝基吡吡吡嗪-1-氧化物（LLM-105）中的溶解度的测量，相关性和热力学溶剂中的溶剂</span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/academic-conference-foreign_meeting-202524_thesis/020513888748.html">Microreactor flow synthesis of the secondary high explosive 2,6-diamino-3,5-dinitropyrazine-1 -oxide (LLM-105)</a> <b>[C]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Nathaniel B. 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2021</span><span>,第003期</span> </span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/academic-journal-cn_chinese-journal-energetic-materials_thesis/0201227055839.html">3,5-二氨基-2,6-二硝基吡嗪-1-氧化物合成及性能</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=王帜&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 王帜</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=张文全&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,张文全</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=王康才&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,王康才</a> <span> <a href="/journal-cn-8325/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 含能材料 </a> </span> <span> . 2016</span><span>,第008期</span> </span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/academic-journal-cn_acta-armamentarii_thesis/0201226910470.html">重结晶方法对2,6-二氨基-3,5-二硝基吡嗪-1-氧化物晶体特性及性能影响</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=徐容&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 徐容</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=廖龙渝&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,廖龙渝</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=王述存&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,王述存</a> <span> <a href="/journal-cn-8314/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 兵工学报 </a> </span> <span> . 2015</span><span>,第011期</span> </span> </div> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/academic-journal-cn_chinese-journal-inorganic-chemistry_thesis/0201250699706.html">两个2,6-二氨基-3,5-二硝基吡嗪-1-氧化物含能配合物的合成、晶体结构及催化性能</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=刘进剑&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 刘进剑</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=刘祖亮&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,刘祖亮</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=成健&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,成健</a> <span> <a href="/journal-cn-15070/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 无机化学学报 </a> </span> <span> . 2014</span><span>,第003期</span> </span> </div> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/academic-journal-cn_journal-chemical-engineering-chinese-universities_thesis/0201233223108.html">2,6-二氨基-3,5-二硝基吡嗪-1-氧化物合成及爆炸性质研究</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=赵晓锋&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 赵晓锋</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=刘祖亮&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,刘祖亮</a> <span> <a href="/journal-cn-11277/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 高校化学工程学报 </a> </span> <span> . 2013</span><span>,第002期</span> </span> </div> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-22400_thesis/02022614161.html">2,6-二氨基-3,5-二硝基吡嗪-1-氧化物(LLM-105)的热性能及其在推进剂中的应用研究</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=高红旭&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 高红旭</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=赵凤起&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,赵凤起</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=仪建华&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,仪建华</a> <span> <a href="/conference-cn-22400/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 中国宇航学会固体火箭推进24届年会 </a> <span> <span> . 2007</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020313015839.html">2,6-二氨基-3,5-二硝基吡嗪-1-氧化物合成工艺优化</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=王金敏&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 王金敏</a> <span> . 2016</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06120704152.html">用于在宽操作温度范围内除去氮氧化物和二氧芑的包含天然锰矿的钒/二氧化钛催化剂和使用该催化剂的方法</a> <b>[P]</b> . <span> 中国专利： CN101300068B </span> <span> . 2010.12.15</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120105499413.html">用于在宽操作温度范围内除去氮氧化物和二氧芑的包含天然锰矿的钒/二氧化钛催化剂和使用该催化剂的方法</a> <b>[P]</b> . <span> 中国专利： CN101300068A </span> <span> . 2008-11-05</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130427211584.html">SYNTHESIS OF PYRAZINES INCLUDING 2,6-DIAMINOPYRAZINE-1-OXIDE (DAPO) AND 2,6-DIAMINO-3,5-DINITROPYRAZINE-1-OXIDE (LLM-105)</a> <b>[P]</b> . <span> 外国专利： <!-- 世界知识产权组织专利： --> WO2010123806A1 </span> <span> . 2010-10-28</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：包括2,6-二氨基吡嗪-1-氧化物（DAPO）和2,6-二氨基-3,5-二硝基吡嗪-1-氧化物（LLM-105）的吡嗪的合成 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130428451319.html">SYNTHESIS OF PYRAZINES INCLUDING 2,6-DIAMINOPYRAZINE-1-OXIDE (DAPO) AND 2,6-DIAMINO-3,5-DINITROPYRAZINE-1-OXIDE (LLM-105)</a> <b>[P]</b> . <span> 外国专利： <!-- 美国专利： --> US2010267955A1 </span> <span> . 2010-10-21</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：包括2,6-二氨基吡嗪-1-氧化物（DAPO）和2,6-二氨基-3,5-二硝基吡嗪-1-氧化物（LLM-105）的吡嗪的合成 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130428133103.html">New synthesis of 2,6-diamino-3,5-dinitropyrazine-1-oxide from 2,6-diaminopyrazine-1-oxide</a> <b>[P]</b> . <span> 外国专利： <!-- 美国专利： --> US2009299067A1 </span> <span> . 2009-12-03</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：由2,6-二氨基吡嗪-1-氧化物新合成2,6-二氨基-3,5-二硝基吡嗪-1-氧化物 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" 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