Cycloadducts of Methyl Hydroxyalkynoates and DBU: Transformation into Tethered Furan-2(5H)-one and Caprolactam Structures

Trofimov B. A.; Shemyakina O. A.; Stepanov A. V.; Volostnykh O. G.; Malkina A. G.

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Cycloadducts of Methyl Hydroxyalkynoates and DBU: Transformation into Tethered Furan-2(5H)-one and Caprolactam Structures

机译：甲基羟基炔酸酯和DBU的环形加成：转化成束呋喃-2（5H） - 酮和己内酰胺结构

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Cycloadducts of 1,8-diazabicyclo[5.4.0] undec-7-ene and methyl 4-hydroxyalk-2-ynoates, octahydro-5H, 9H-[1,3] oxazolo[2', 3' : 2,3] pyrimido[1,2-a] azepines, in the presence of potassium hydroxide in aqueous ethanol were converted to structures in which furan-2(5H)-one and caprolactam rings are linked to each other through an aminopropane tether.

机译：1,8-diazabodicclo的环形加廊[5.4.0] UDEC-7-ENE和甲基4-羟基烷基-2-炔酸盐，八氢镍-5H，9H- [1,3]恶唑[2'，3'：2,3] 嘧啶[1,2-A]偶氮胺在乙醇水溶液中的存在下转化为呋喃-2（5h） - 酮和己内酰胺环通过氨基丙烷系绳彼此连接。

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《Russian Journal of Organic Chemistry》 |2017年第12期|共3页
作者
Trofimov B. A.; Shemyakina O. A.; Stepanov A. V.; Volostnykh O. G.; Malkina A. G.;
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Russian Acad Sci Favorskii Irkutsk Inst Chem Siberian Branch Ul Favorskogo 1 Irkutsk 664033 Russia;

Russian Acad Sci Favorskii Irkutsk Inst Chem Siberian Branch Ul Favorskogo 1 Irkutsk 664033 Russia;

Russian Acad Sci Favorskii Irkutsk Inst Chem Siberian Branch Ul Favorskogo 1 Irkutsk 664033 Russia;

Russian Acad Sci Favorskii Irkutsk Inst Chem Siberian Branch Ul Favorskogo 1 Irkutsk 664033 Russia;

Russian Acad Sci Favorskii Irkutsk Inst Chem Siberian Branch Ul Favorskogo 1 Irkutsk 664033 Russia;

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中图分类有机化学;
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1. Cycloadducts of Methyl Hydroxyalkynoates and DBU: Transformation into Tethered Furan-2(5H)-one and Caprolactam Structures [J] . Trofimov B. A., Shemyakina O. A., Stepanov A. V., Russian Journal of Organic Chemistry . 2017,第12期

机译：甲基羟基炔酸酯和DBU的环形加成：转化成束呋喃-2（5H） - 酮和己内酰胺结构
2. Nano-colloidal silica-tethered polyhedral oligomeric silsesquioxanes with eight branches of 3-aminopropyltriethoxysilane as high performance catalyst for the preparation of furan-2(5H)-ones [J] . Hossein Shahbazi-Alavi, Javad Safaei-Ghomi Nanochemistry Research . 2019,第1期

机译：具有3-氨基丙基三乙氧基硅烷的八个分支的纳米胶体二氧化硅束缚的多面体低聚倍半硅氧烷作为制备呋喃-2（5H）-一的高性能催化剂
3. Sonosynthesis of furan-2(5H)-ones using nanosilica-tethered polyhedral oligomeric silsesquioxanes [J] . Shahbazi-Alavi Hossein, Khojasteh-Khosro Sheida, Safaei-Ghomi Javad, Journal of the Iranian Chemical Society . 2019,第11期

机译：呋喃-2（5H） - 使用纳米单乳束多面体低聚硅氧烷硅氧烷的呋喃-2（5H）的旋转性
4. (5S)-3-Chloro-5-(1R2S5R)-2-isopropyl-5-methylcyclohexyloxy-4-(4-methylpiperidin-1-yl)furan-2(5H)-one [O] . Xiao-Mei Wang, Jian-Hua Fu, Song-Liang Cai, 2011

机译：（5S）-3-氯-5-（1R2S5R）-2-异丙基-5-甲基环己基氧基 -4-（4-甲基哌啶-1-基）呋喃-2（5H）-
5. (5S)-3-Chloro-5-[(1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy]-4-(4-methylpiperidin-1-yl)furan-2(5H)-one [O] . Wang, Xiao-Mei, Fu, Jian-Hua, Cai, Song-Liang, 2011

机译：（5S）-3-氯-5-[（1R，2S，5R）-2-异丙基-5-甲基环己基氧基] -4-（4-甲基哌啶-1-基）呋喃-2（5H）-

Cycloadducts of Methyl Hydroxyalkynoates and DBU: Transformation into Tethered Furan-2(5H)-one and Caprolactam Structures

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