Heterocyclization of 5-(Arylmethylidene)pyrimidine-2,4,6(1H,3H,5H)-triones with Arenecarbaldehyde Oximes in the Presence of N-Bromosuccinimide and Triethylamine

Tyrkov A. G.; Yurtaeva E. A.

首页> 外文期刊>Russian Journal of Organic Chemistry >Heterocyclization of 5-(Arylmethylidene)pyrimidine-2,4,6(1H,3H,5H)-triones with Arenecarbaldehyde Oximes in the Presence of N-Bromosuccinimide and Triethylamine

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Heterocyclization of 5-(Arylmethylidene)pyrimidine-2,4,6(1H,3H,5H)-triones with Arenecarbaldehyde Oximes in the Presence of N-Bromosuccinimide and Triethylamine

机译：在N-溴代琥珀酰亚胺和三乙胺存在下，用仲二甲醛肟和三乙胺与仲二甲醛肟的5-（芳基甲基）嘧啶-2,4,6（1H，3H，5H）的杂环化

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摘要

5-(Arylmethylidene)pyrimidine-2,4,6(1H,3H,5H)-triones reacted with substituted benzaldehyde oximes in the presence of N-bromosuccinimide and triethylamine to give 1,4-diaryl-2-oxa-3,7,9-triazaspiro-[4.5]dec-3-ene-6,8,10-triones and 3,4-diaryl-1,2,5-oxadiazole N-oxides.

机译：5-（芳基甲基）嘧啶-2,4,6（1H，3H，5H） - 在N-溴代琥珀酰亚胺和三乙胺存在下与取代的苯甲醛肟反应，得到1,4-二芳基-2-Oxa-3,7 ，9-Triazaspiro-[4.5] Dec-3-Ene-6,8,10- Triones和3,4-二芳基-1,2,5-恶二唑N-氧化物。

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来源
《Russian Journal of Organic Chemistry》 |2019年第7期|共5页
作者
Tyrkov A. G.; Yurtaeva E. A.;
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作者单位

Astrakhan State Univ Astrakhan Russia;

Volgograd State Med Univ Pyatigorsk Med &

Pharmaceut Inst Branch Pyatigorsk Russia;

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正文语种 eng
中图分类有机化学;
关键词
5-(arylmethylidene)pyrimidine-2; 4; 6(1H; 3H; 5H)-triones; arenecarbaldehyde oximes; 1; 3-dipolar cycloaddition; N-bromosuccinimide; triethylamine; 1; 4-diaryl-2-oxa-3; 7; 9-triazaspiro4.5dec-3-ene-6; 8; 10-triones; 3; 4-diaryl-1; 2; 5-oxadiazole N-oxides;

机译：5-（芳基甲基）嘧啶-2;4;6（1H;3小时;5H） - 仲赤醛肟;1;3-偶极环加成;N-溴嘧啶;三乙胺;1;4-二芳基-2-牛皮酰亚胺;7;9-Triazaspiro [4.5] Dec-3-Ene-6;8;10-三件;3;4-二芳基-1;2;5-氧代唑N-氧化物;

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1. Heterocyclization of 5-(Arylmethylidene)pyrimidine-2,4,6(1H,3H,5H)-triones with Arenecarbaldehyde Oximes in the Presence of N-Bromosuccinimide and Triethylamine [J] . Tyrkov A. G., Yurtaeva E. A. Russian Journal of Organic Chemistry . 2019,第7期

机译：在N-溴代琥珀酰亚胺和三乙胺存在下，用仲二甲醛肟和三乙胺与仲二甲醛肟的5-（芳基甲基）嘧啶-2,4,6（1H，3H，5H）的杂环化
2. Synthesis and Antimycobacterial Activity of 5-(Hetarylmethylidene)-2,4,6-Pyrimidine-2,4,6(1H,3H,5H )-Triones And 5-(2-Chloropropylidene)-2,4,6-Pyrimidine-2,4,6(1H,3H,5H )-Triones [J] . Yushin M. Yu, Tyrkov A. G., Saroyants L. V, Pharmaceutical Chemistry Journal . 2020,第2期

机译：5-（hetarylmethylynylynylynidine-2,4,6（1H，3H，5H） - 十字和5-（2-氯丙烯）-2,4,6-嘧啶 - 的合成和抗致细胞活性 - 2,4,6（1h，3h，5h） - 轴
3. Three-component heterocyclization of 5-(arylmethylidene)pyrimidine-2,4,6(1H,3H,5H)-triones with aldehydes and amino acids [J] . Tyrkov A. G., Yurtaeva E. A., Dankova L. A. Russian Journal of Organic Chemistry . 2017,第7期

机译：用醛和氨基酸为5-（芳基甲基）嘧啶-2,4,6（1H，3H，5H）的三分 - （芳基甲基）嘧啶-2,4,6（1H，3H，5H）的三分 - 组分杂环化
4. Glassy 2-(1-benzyl-2-styryl-6-methylpyridin-4(1-H)-ylidene) fragment containing 1H-indene-1,3(2H)-dione and pyrimidine-2,4,6(1H,3H,5H)-trione derivatives with light-emitting and amplified spontaneous emission properties [C] . Elmars Zarins, Julija Pervenecka, Elina Misina, Conference on Fiber Lasers and Glass Photonics: Materials through Applications . 2020

机译：含1H-茚-1,3（2H）-二酮和嘧啶-2,4,6（1H）的玻璃状2-（1-苄基-2-苯乙烯基-6-甲基吡啶-4（1-H）-亚烷基）片段具有发光和放大的自发发射特性的3H，5H）-三酮衍生物
5. Novel substituted (Z)-5-((N-benzyl-1H-indol-3-yl)methylene)imidazolidine-2,4-diones and 5-((N-benzyl-1H-indol-3-yl)methylene)pyrimidine-2,4,6(1H,3H,5H)-triones as potent radio-sensitizing agents [O] . Y. Thirupathi Reddy, Konjeti R. Sekhar, Nidhish Sasi, 2010

机译：新型取代（Z）-5 - （（N-苄基-1H-吲哚-3-基）亚甲基）咪唑烷-2,4-二乙酯和5-（（N-苄基-1H-吲哚-3-基）亚甲基）嘧啶-2,4,6（1H，3H，5H） - 标纹作为有效的无线电敏化剂
6. Results of a Local Lymph Node Assay in Mice (LLNA/IMDS) with Toluene Diisocyanate based adduct in Organic Solvent (TDI Trimer) 1,3,5-Triazine- 2,4,6(1H,3H,5H)-trione, 1,3,5-tris(3-isocya natomethylphenyl). [R] . 2011

机译：基于甲苯二异氰酸酯的有机溶剂加成物（TDI三聚体）1,3,5-三嗪-2,4,6（1H，3H，5H） - 三酮，1小鼠局部淋巴结检测结果（LLNa / ImDs），3,5-三（3-isocya natomethylphenyl）。

Heterocyclization of 5-(Arylmethylidene)pyrimidine-2,4,6(1H,3H,5H)-triones with Arenecarbaldehyde Oximes in the Presence of N-Bromosuccinimide and Triethylamine

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