Palladium-catalyzed synthesis of pyrimido[5 ',4 ':3,4]pyrrolo[1,2-f]phenanthridine-12, 14(11H,13H)-diones and related compounds

Shevchenko M. A.; Tkachenko Y. N.; Astakhov A. V.; Khazipov O. V.; Tyurin R. V.; Pasyukov D. V.; Tafeenko V. A.; Kravchenko O. A.; Chernyshev V. M.

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Palladium-catalyzed synthesis of pyrimido[5 ',4 ':3,4]pyrrolo[1,2-f]phenanthridine-12, 14(11H,13H)-diones and related compounds

机译：钯催化合成嘧啶[5'，4'：3,4] Pyrrolo [1,2-F]菲啶-12,14（11h，13h） - 二酮和相关化合物

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摘要

Representatives of the new heterocyclic system, pyrimido[5',4':3,4]pyrrolo[1,2-f]phenanthridine, were obtained via the intramolecular C-H-arylation of 6-aryl-5-(2-bromophenyl) pyrrolo[3,4-d]pyrimidine-2,4-diones catalyzed by palladium complexes with N-heterocyclic carbene ligands (Pd/NHC).

机译：通过6-芳基-5-（2-溴苯基）Pyrrolo的分子内Ch-芳基，获得新的杂环体系，嘧啶[5'，4'：3,4]吡咯并[5'，4'：3,4] Pyrrolo [1,2-F]菲利丁 [3,4-D]氟酰胺-2,4-二酮，钯配合物用N-杂环碳配体（Pd / NHC）催化。

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来源
《Russian Chemical Bulletin》 |2018年第9期|共11页
作者
Shevchenko M. A.; Tkachenko Y. N.; Astakhov A. V.; Khazipov O. V.; Tyurin R. V.; Pasyukov D. V.; Tafeenko V. A.; Kravchenko O. A.; Chernyshev V. M.;
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作者单位

Platov South Russian State Polytech Univ NPI 132 Ul Prosveshcheniya Novocherkassk 346428 Russia;

Southern Fed Univ 7 Ul Zorge Rostov Na Donu 344090 Russia;

Platov South Russian State Polytech Univ NPI 132 Ul Prosveshcheniya Novocherkassk 346428 Russia;

Platov South Russian State Polytech Univ NPI 132 Ul Prosveshcheniya Novocherkassk 346428 Russia;

Platov South Russian State Polytech Univ NPI 132 Ul Prosveshcheniya Novocherkassk 346428 Russia;

Platov South Russian State Polytech Univ NPI 132 Ul Prosveshcheniya Novocherkassk 346428 Russia;

Lomonosov Moscow State Univ 1 Leninskie Gory Moscow 119991 Russia;

Platov South Russian State Polytech Univ NPI 132 Ul Prosveshcheniya Novocherkassk 346428 Russia;

Platov South Russian State Polytech Univ NPI 132 Ul Prosveshcheniya Novocherkassk 346428 Russia;

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正文语种 eng
中图分类化学;
关键词
pyrimido5 '; 4 ':3; 4pyrrolo1-2-fphenanthridines; pyrrolo3; 4-dpyrimidines; cyclization; C-H-activation; arylation; palladium; N-heterocyclic carbenes; catalysis;

机译：Pyrimido [5';4'：3;4] Pyrrolo [1-2-F]菲尼因植物;吡咯啉[3;4-D]嘧啶;环化;C-H活化;芳基化;钯;钯;N-杂环碳;催化;

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1. Palladium-catalyzed synthesis of pyrimido[5 ',4 ':3,4]pyrrolo[1,2-f]phenanthridine-12, 14(11H,13H)-diones and related compounds [J] . Shevchenko M. A., Tkachenko Y. N., Astakhov A. V., Russian Chemical Bulletin . 2018,第9期

机译：钯催化合成嘧啶[5'，4'：3,4] Pyrrolo [1,2-F]菲啶-12,14（11h，13h） - 二酮和相关化合物
2. Палладий-катализируемый синтез пиримидо[5',4':3,4]пирроло[1,2-У]фенантридин-12,14(11H,13H)-дионов и родственных соединений [J] . М. А. Шевченко, Ю. Н. Ткаченко, А. В. Астахов Известия Аκадемии науκ. Серия Химичесκая . 2018,第9期

机译：钯催化合成嘧啶[5'，4'，4'，3,4]吡咯洛[1,2-Y]芬顿吖啶-12.14（11h，13h） - 和相关的化合物
3. Pyrrolo(3,4-c)quinoline-1,3-diones as potent caspase-3 inhibitors. Synthesis and SAR of 2-substituted 4-methyl-8-(morpholine-4-sulfonyl)-pyrrolo(3,4-c)quinoline-1,3-diones. [J] . Kravchenko DV, Kysil VM, Tkachenko SE, European Journal of Medicinal Chemistry: Chimie Therapeutique . 2005,第12期

机译：Pyrrolo（3,4-c）quinoline-1,3-diones作为有效的caspase-3抑制剂。 2-取代的4-甲基-8-（吗啉-4-磺酰基）-吡咯并（3,4-c）喹啉-1,3-二酮的合成和SAR。
4. SYNTHESIS OF OCTAHYDRO-PYRROLO3,4-b-PIPIREDIN-2-ONES, OCTAHYDRO-PYRROLO3,4-bAZEPIN-2-ONES AND REACTIONS WITH THEM(Abstracts) [C] . Valery S Kochubey, Oleg M Shamaev, Oleg G Rodin European Symposium on Organic Chemistry . 2007

机译：八氢盐 - 吡咯的合成3,4-B - 哌啶-2-吡咯3,4-B偶氮二蛋白-2-β-2 - 与它们（摘要）
5. I. Reactivity of electron deficient indoles toward nucleophiles, Diels-Alder reactions and dipolar cycloadditions. II. Synthesis of pyrrolo[3,4-b]indoles. [D] . Kishbaugh, Tara Lynn Sanders. 2003

机译：I.缺电子的吲哚对亲核试剂，Diels-Alder反应和偶极环加成反应。二。吡咯并[3，4-b]吲哚的合成。
6. (3aR,6aR)-1-Phenyl-5-[(R)-1-phenylethyl]-3-[4-(trifluoromethyl)phenyl]-1,6a-dihydropyrrolo[3,4-c]pyrazole-4,6(3aH,5H)-dione [O] . Chris F. Fronczek, Yaşar Dürüst, Muhammet Yildirim, 2016

机译：（3aR，6aR）-1-苯基-5-[（R）-1-苯乙基] -3- [4-（三氟甲基）苯基] -1,6a-二氢吡咯并[3,4-c]吡唑-4,6 （3aH，5H）-二酮
7. Pyrimidine derivatives and related compounds. XXXIII. Reactions of 6-bromomethyl-5-formyl-1,3-dimethyluracil and its hydrazones with nucleophiles. Synthesis of pyrrolo(3,4-d)pyrimidines and pyrimido(4,5-d)pyridazines. [O] . KOSAKU HIROTA, YOSHIHIRO YAMADA, TETSUJI ASAO, 1981

机译：嘧啶衍生物和相关化合物。 xxxiii。 6-溴甲基-5-甲酰基-1,3-二甲基脲及其与亲核试剂的反应。吡咯醇（3,4-D）嘧啶和嘧啶（4,5-D）吡啶啶的合成。

Palladium-catalyzed synthesis of pyrimido[5 ',4 ':3,4]pyrrolo[1,2-f]phenanthridine-12, 14(11H,13H)-diones and related compounds

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