Chiral determination of cinchonine using an electrochemiluminescent sensor with molecularly imprinted membrane on the surfaces of magnetic particles

机译：用电化学发光传感器在磁性颗粒表面上使用电化学发光传感器的手性测定Cinchonine

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Abstract > A novel molecular imprinting electrochemiluminescence sensor for detecting chiral cinchonine molecules was developed with a molecularly imprinted polymer membrane on the surfaces of magnetic microspheres. Fe <sub>3</sub> O <sub>4</sub> @Au nanoparticles modified with 6‐mercapto‐beta‐cyclodextrin were used as a carrier, cinchonine as a template molecule, methacrylic acid as a functional monomer and N , N ′‐methylenebisacrylamide as a cross‐linking agent. Cinchonine was specifically recognized by the 6‐mercapto‐beta‐cyclodextrin functional molecularly imprinted polymer and detected based on enhancement of the electrochemiluminescence intensity caused by the reaction of tertiary amino structures of cinchonine molecules with Ru(bpy) <sub>3</sub> 2+ . Cinchonine concentrations of 1?×?10 ?10 to 4?×?10 ?7 ?mol/L showed a good linear relationship with changes of the electrochemiluminescence intensity, and the detection limit of the sensor was 3.13?×?10 ?11 ?mol/L. The sensor has high sensitivity and selectivity, and is easy to renew. It was designed for detecting serum samples, with recovery rates of 98.2% to 107.6%. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“main”> <标题类型=“main”>摘要</标题> >用于检测手性融合分子的新型分子印迹电化学传感器，在磁性微球表面上用分子印迹聚合物膜进行显影。用6-巯基 - β-环糊精改性的Fe <sub> 3 </ sub> O <sub> 4 </ sub> @au纳米粒子用作载体，Cinchonine作为模板分子，甲基丙烯酸作为官能单体和< I> n / i>， n </ i>' - 亚甲基异丙酰胺作为交联剂。 Chicchonine由6-巯基 - β-环糊精功能的分子印迹聚合物特异性识别，并基于由Ru（BPY）<sub> 3 </ sub>的亚氨基结构反应引起的电化学发光强度的增强来检测。 2 + </ sup>。 Conchonine浓度为1？×10 α10</ sup>至4？×10 Δ7</ sup>？mol / l与电化学发光强度的变化显示出良好的线性关系，以及传感器的检测极限为3.13？×10 ？11 </ sup>？mol / l。传感器具有高灵敏度和选择性，并且易于更新。它设计用于检测血清样品，恢复率为98.2％至107.6％。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-26441/'>《Luminescence: The journal of biological and chemical luminescence》</a> <b style="margin: 0 2px;">|</b><span>2017年第7期</span><b style="margin: 0 2px;">|</b><span>共7页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yuan Xingyi&option=202" target="_blank" rel="nofollow">Yuan Xingyi;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Tan Yanji&option=202" target="_blank" rel="nofollow">Tan Yanji;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wei Xiaoping&option=202" target="_blank" rel="nofollow">Wei Xiaoping;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li Jianping&option=202" target="_blank" rel="nofollow">Li Jianping;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Guangxi Geoenvironmental Monitoring StationGuilin China;</p> <p>Guangxi Geoenvironmental Monitoring StationGuilin China;</p> <p>College of Chemistry and BioengineeringGuilin University of TechnologyGuilin China;</p> <p>College of Chemistry and BioengineeringGuilin University of TechnologyGuilin China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1345.html" title="生物光学">生物光学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=chiral molecule&option=203" rel="nofollow">chiral molecule;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=cinchonine&option=203" rel="nofollow">cinchonine;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=electrochemiluminescence&option=203" rel="nofollow">electrochemiluminescence;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Fe 3 O 4 @Au&option=203" rel="nofollow">Fe 3 O 4 @Au;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=molecular imprinting technique&option=203" rel="nofollow">molecular imprinting technique;</a> </p> <div class="translation"> 机译：手性分子;Cinchonine;电化学发光;Fe 3 O 4 @au;分子印迹技术; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704023986309.html">Chiral determination of cinchonine using an electrochemiluminescent sensor with molecularly imprinted membrane on the surfaces of magnetic particles</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yuan Xingyi&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Yuan Xingyi,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Tan Yanji&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Tan 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