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HPLC?EC Analysis of Estrogenic Compounds: A Comparison of Diamond and Tetrahedral Amorphous Carbon Electrode Performance

机译：HPLCα雌性化合物的EC分析：金刚石和四面体无定形碳电极性能的比较

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Abstract > High pressure liquid chromatography (HPLC) with amperometric detection was used to quantify estrogenic compounds in water samples. The main goal was to compare the detection figures of merit for boron‐doped diamond thin‐film (BDD) and nitrogen‐incorporated tetrahedral amorphous carbon (t a ‐C?:?N) thin‐film electrodes. The target analytes were estrone, estradiol, and estriol. The BDD and t a ‐C?:?N electrodes were investigated because of their excellent properties, which include a wide potential window, low background current, microstructural stability at high potentials, low limits of detection, weak molecular adsorption, fouling resistance and response reproducibility. t a ‐C?:?N electrodes have not yet been investigated extensively in electroanalysis and are receiving increasing interest because they exhibit many of the excellent electrochemical properties of BDD electrodes and they can be deposited at room temperature by physical vapor deposition. The results reveal as low or lower background current and noise for the t a ‐C?:?N electrode, as compared to the BDD electrode, and comparable or superior analytical detection figures of merit for all three emerging pollutants. The linear dynamic range for both electrodes was from 0.2 to 100?μmol?L ?1 for estriol, and 0.4 to 100?μmol?L ?1 for estradiol and estrone, and the sensitivity ranged from 9.1 to 11.2?mA?mol?L ?1 . For all three analytes, the limit of detection (S/N=3) ranged from 0.16–0.35?μmol?L ?1 (45‐95?ppb) for BDD and 0.20–0.34?μmol?L ?1 (58‐95?ppb) for t a ‐C?:?N. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>摘要</标题> >高压液相色谱（HPLC）与安培检测用于量化水样中的雌激素化合物。主要目标是比较硼掺杂金刚石薄膜（BDD）的优点的检测图和氮气掺入的四面体无定形碳（T <I> A </ I> -C→：Δn）薄膜电极。靶分析物是雌激素，雌二醇和雌醇。 BDD和T <I> -C？：Δn电极是由于它们的优异性能而研究，包括宽势窗口，高电位，微观结构稳定性，在高电位下，低势，检测限差，弱分子吸附，污垢抗性和反应再现性。 t a </ i> -c？：尚未在电分析中广泛研究电极，并且由于它们表现出BDD电极的许多优异的电化学性质，并且它们可以在室温下沉积出来的许多优异的兴趣物理气相沉积。结果显示为T <I> A </ I> -C的低或更低的背景电流和噪声，与BDD电极相比，与BDD电极相比，所有三个新兴的可比分析检测数据污染物。对于雌二醇，两个电极的线性动态范围为0.2至100Ω·μmol？l β1</ sup>，雌二醇和雌二酮，并且灵敏度范围从9.1到11.2？ma？mol？l ？1 </ sup>。对于所有三个分析物，检测极限（S / N = 3）的范围为0.16-0.35Ωμmol？l （45-95→ppb），用于Bdd和0.20-0.34Ωμmol？ l ？1 </ sup>（58-95？ppb）用于t a </ i> -c？：？n。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-22546/'>《Electroanalysis》</a> <b style="margin: 0 2px;">|</b><span>2018年第7期</span><b style="margin: 0 2px;">|</b><span>共8页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Aigaje?Espinosa Elizabeth K.&option=202" target="_blank" rel="nofollow">Aigaje?Espinosa Elizabeth K.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Qiu Joy&option=202" target="_blank" rel="nofollow">Qiu Joy;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Jaro?ová Romana&option=202" target="_blank" rel="nofollow">Jaro?ová Romana;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Castiaux Andre&option=202" target="_blank" rel="nofollow">Castiaux Andre;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Swain Greg M.&option=202" target="_blank" rel="nofollow">Swain Greg M.;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Faculty of Chemical Engineering and Agro-IndustryLadrón de Guevara E11-253 Escuela Politécnica Nacional Quito 170525 Ecuador;</p> <p>High School Honors Science Program (HSHSP)Michigan State UniversityEast Lansing MI 48824 USA;</p> <p>Department of ChemistryMichigan State UniversityEast Lansing MI 48824 USA;</p> <p>Department of ChemistryMichigan State UniversityEast Lansing MI 48824 USA;</p> <p>Department of ChemistryMichigan State UniversityEast Lansing MI 48824 USA;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/4817.html" title="电化学、电解、磁化学">电化学、电解、磁化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Boron-droped diamond electrode&option=203" rel="nofollow">Boron-droped diamond electrode;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=tetrahedral amorphous carbon electrode&option=203" rel="nofollow">tetrahedral amorphous carbon electrode;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=estrogenic compounds&option=203" rel="nofollow">estrogenic compounds;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=high performance liquid chromatography&option=203" rel="nofollow">high performance liquid chromatography;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=amperometric detection&option=203" rel="nofollow">amperometric detection;</a> </p> <div class="translation"> 机译：硼化金刚石电极;四面体非晶碳电极;雌激素化合物;高效液相色谱;安培检测; 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initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：像四面体钻石一样的非晶碳的掺杂 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" style="bottom: 19px;z-index: 999;" onclick="ywcd('0704023174731','4',7,2,1,'',this,24)" class="delivery" prompt="010401" title="通过人工服务将文献原文发送至邮箱" >获取原文</div> <div class="journalsub-pop-up" style="display: none"> <div class="journal-sub"> <h2>期刊订阅</h2> <img src="https://cdn.zhangqiaokeyan.com/img/loginclose.png" alt="" onclick="$('.journalsub-pop-up').hide()"> <p class="pardon">抱歉，该期刊暂不可订阅，敬请期待！</p> <p class="current">目前支持订阅全部北京大学中文核心（2020）期刊目录。</p> <div 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