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Preparation and Microwave Absorption Properties of Polyaniline and Magnetite Core-Shell-Structured Hybrid

机译:聚苯胺和磁铁矿纤维壳结构杂种的制备和微波吸收性能

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摘要

In this study, polyaniline and Fe3O4 (PAN@Fe3O4) hybrids are fabricated and their microwave absorption property is studied. PAN@Fe3O4 hybrids are fabricated by the in situ aniline polymerization at spherical of Fe3O4 which is prepared by the solvothermal process. Fourier-transform infrared spectrophotometer (FTIR), X-ray diffraction (XRD), and X-ray photoelectron spectroscopy (XPS) are applied to confirm the composition of the fabricated PAN@Fe3O4 hybrids. The morphologies of PAN@Fe3O4 hybrids are studied by scanning electron microscope (SEM) and transmission electron microscopy (TEM). The content of polyaniline in the PAN@Fe3O4 hybrids is calculated by thermogravimetric analysis (TGA). The magnetic properties of PAN@Fe3O4 hybrids are characterized by vibrating sample magnetometer (VSM). The microwave absorption property of PAN@Fe3O4 hybrids are measured on a vector network analyzer. The research show that the microwave absorptions property of the obtained PAN@Fe3O4 hybrids can be adjusted by controlling the in situ aniline polymerization at spherical of Fe3O4.
机译:在该研究中,制造聚苯胺和Fe3O4(PAN @ Fe3O4)杂种,并研究了它们的微波吸收性能。 PAN @ Fe3O4杂交物由在Fe3O4的球形上的原位苯胺聚合制备,其通过溶剂热法制备。傅里叶变换红外分光光度计(FTIR),X射线衍射(XRD)和X射线光电子能谱(XPS)用于确认制造的PAN @ Fe3O4杂交种的组成。通过扫描电子显微镜(SEM)和透射电子显微镜(TEM)研究了PAN @ Fe3O4杂种的形态。 PAN @ Fe3O4杂交体中聚苯胺的含量通过热重分析(TGA)计算。 PAN @ FE3O4杂交物的磁性特征在于振动样品磁力计(VSM)。在向量网络分析仪上测量PAN @ FE3O4混合动力车的微波吸收性能。该研究表明,通过控制Fe3O4球形的原位苯胺聚合来调节所得PAN @ Fe3O4杂种的微波吸收性能。

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