Enhancement of Wetting and Mechanical Properties of UHMWPE‐Based Composites through Alumina Atomic Layer Deposition

Shimel Meni; Gouzman Irina; Grossman Eitan; Barkay Zahava; Katz Sari; Bolker Asaf; Eliaz Noam; Verker Ronen

摘要

Abstract >Ultrahigh molecular weight polyethylene (UHMWPE) fibers suffer from poor adhesion to polar matrices in composites due to their chemically inert surface, thus limiting the use of UHMWPE‐based fabrics and composites. Atomic layer deposition (ALD) is a useful method of constructing a thin oxide layer, with a variety of oxides available, enabling a nondestructive method for surface modification. Here, UHMWPE fibers and fabrics are coated by ALD with a thin alumina layer, using two precursors—trimethylaluminum (TMA) and water—to a final coating thickness of 39 nm. The effect of the oxide coating layer is determined by various mechanical and physical tests. The contact angle is reduced by 44–49%, indicating a substantial increase in wettability. Significant improvements are observed in the flexural modulus, flexural strength, interlaminar shear strength, resilience, and toughness. Frequency dependence tests show an improvement in storage modulus at all tested frequencies, insinuating higher impact toughness at high strain rates. Failure analysis reveals a change in the failure mode, from pinholes formation and adhesion failure to cohesion failure and mixed failure modes. Thus, the use of ALD alumina‐coated UHMWPE fibers in composites shows high scientific and technological potential. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> >超高分子量聚乙烯（UHMWPE）纤维由于其化学惰性表面而患有复合材料中的极性基质的粘附性差，因此限制了基于UHMWPE的织物和复合材料的使用。原子层沉积（ALD）是构建薄氧化物层的有用方法，其具有可用各种氧化物，使得表面改性的非破坏方法。这里，UHMWPE纤维和织物通过ALD用薄氧化铝层涂覆，使用两个前体 - 三甲基铝（TMA）和水至终涂层厚度为39nm。通过各种机械和物理测试确定氧化物涂层的效果。接触角减少44-49％，表明润湿性大幅增加。在弯曲模量，弯曲强度，层间剪切强度，弹性和韧性中观察到显着改进。频率依赖性试验显示所有测试频率的储存模量的改善，在高应变率下呈现更高的冲击韧性。故障分析显示出故障模式的变化，从针孔形成和粘合性发生故障到粘合性故障和混合衰竭模式。因此，在复合材料中使用ALD氧化铝涂覆的UHMWPE纤维显示出高的科学和技术潜力。</ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-18063/'>《Advanced materials interfaces》</a> <b style="margin: 0 2px;">|</b><span>2018年第14期</span><b style="margin: 0 2px;">|</b><span>共9页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Shimel Meni&option=202" target="_blank" rel="nofollow">Shimel Meni;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Gouzman Irina&option=202" target="_blank" rel="nofollow">Gouzman Irina;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Grossman Eitan&option=202" target="_blank" rel="nofollow">Grossman Eitan;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Barkay Zahava&option=202" target="_blank" rel="nofollow">Barkay Zahava;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Katz Sari&option=202" target="_blank" rel="nofollow">Katz Sari;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Bolker Asaf&option=202" target="_blank" rel="nofollow">Bolker Asaf;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Eliaz Noam&option=202" target="_blank" rel="nofollow">Eliaz Noam;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Verker Ronen&option=202" target="_blank" rel="nofollow">Verker Ronen;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Space Environment DepartmentSoreq NRCYavne 81800 Israel;</p> <p>Space Environment DepartmentSoreq NRCYavne 81800 Israel;</p> <p>Space Environment DepartmentSoreq NRCYavne 81800 Israel;</p> <p>Wolfson Applied Materials Research CenterTel‐Aviv UniversityRamat Aviv Tel‐Aviv 6997801 Israel;</p> <p>Space Environment DepartmentSoreq NRCYavne 81800 Israel;</p> <p>Space Environment DepartmentSoreq NRCYavne 81800 Israel;</p> <p>Department of Materials Science and EngineeringTel‐Aviv UniversityRamat Aviv Tel‐Aviv 6997801 Israel;</p> <p>Space Environment DepartmentSoreq NRCYavne 81800 Israel;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/6960.html" title="特种结构材料">特种结构材料;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=composite materials&option=203" rel="nofollow">composite materials;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=functional coatings&option=203" rel="nofollow">functional coatings;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=surface modification&option=203" rel="nofollow">surface modification;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=thin films&option=203" rel="nofollow">thin films;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=UHMWPE&option=203" rel="nofollow">UHMWPE;</a> </p> <div class="translation"> 机译：复合材料;功能涂层;表面改性;薄膜;UHMWPE; </div> </li> </ul> </div> </div> <div class="literature cardcommon" id="literaturereference" style="display:none"> <div class="similarity "> <h3 class="all_title" id="enpatent111">引文网络</h3> <div class="referencetab clearfix"> <ul id="referencedaohang"> <li dataid="referenceul">参考文献</li> <li dataid="citationul">引证文献</li> <li dataid="commonreferenceul">共引文献</li> <li dataid="commoncitationul">同被引文献</li> <li dataid="tworeferenceul">二级参考文献</li> <li dataid="twocitationul">二级引证文献</li> </ul> </div> <div class="reference_details" id="referenceList"> <ul id="referenceul"></ul> <ul id="citationul"></ul> <ul id="commonreferenceul"></ul> <ul id="commoncitationul"></ul> <ul id="tworeferenceul"></ul> <ul id="twocitationul"></ul> </div> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704022434478.html">Enhancement of Wetting and Mechanical Properties of UHMWPE‐Based Composites through Alumina Atomic Layer Deposition</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Shimel Meni&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Shimel Meni,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Gouzman Irina&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Gouzman Irina,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Grossman Eitan&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Grossman Eitan,</a> <a href="/journal-foreign-18063/" target="_blank" rel="nofollow" class="tuijian_authcolor">Advanced materials interfaces .</a> <span>2018</span><span>,第14期</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：通过氧化铝原子层沉积提高UHMWPE基复合材料的润湿性能和力学性能</span> </p> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/070408933535.html">Thermo-mechanical properties of alumina films created using the atomic layer deposition technique</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Miller D.C.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Miller D.C.,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Foster R.R.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Foster R.R.,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Jen S.-H.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Jen S.-H.,</a> <a href="/journal-foreign-28049/" target="_blank" rel="nofollow" class="tuijian_authcolor">Sensors and Actuators, A. 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R.,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext= Jen, S.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> Jen, S.,</a> <span>2010</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：原子层沉积技术制备氧化铝薄膜的热力学性质</span> </p> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/academic-journal-cn_shanghai-plastics_thesis/0201280186020.html">UHMWPE纳米复合材料的制备及力学性能</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=夏晋程&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 夏晋程</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=李志&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,李志</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=叶纯麟&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,叶纯麟</a> <span> <a href="/journal-cn-9191/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 上海塑料 </a> </span> <span> . 2020</span><span>,第002期</span> </span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/academic-journal-cn_china-plastics-industry_thesis/0201271062182.html">SBF氧化降解对辐照交联GO/VE/UHMWPE复合材料结构和力学性能的影响</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=陆佩佩&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 陆佩佩</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=倪自丰&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,倪自丰</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=陈国美&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,陈国美</a> <span> <a href="/journal-cn-9211/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 塑料工业 </a> </span> <span> . 2018</span><span>,第010期</span> </span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/academic-journal-cn_modern-silk-science-technology_thesis/020121635887.html">热处理对UHMWPE短纤纱增强复合材料力学性能的影响</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=马小飞&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 马小飞</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=宋新惠&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,宋新惠</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=张宏妮&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,张宏妮</a> <span> <a href="/journal-cn-9345/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 现代丝绸科学与技术 </a> </span> <span> . 2017</span><span>,第004期</span> </span> </div> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/academic-journal-cn_fiber-reinforced-plasticscomposites_thesis/020127337851.html">CF/UHMWPEF混杂复合材料的力学性能研究</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=张玉芳&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 张玉芳</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=刘海军&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,刘海军</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=庞雅莉&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,庞雅莉</a> <span> <a href="/journal-cn-9515/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 玻璃钢/复合材料 </a> </span> <span> . 2007</span><span>,第004期</span> </span> </div> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/academic-journal-cn_fiber-reinforced-plasticscomposites_thesis/020127359272.html">混杂方式对CF/UHMWPEF混杂复合材料力学性能的影响</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=张用兵&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 张用兵</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=史俊虎&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,史俊虎</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=王利&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,王利</a> <span> <a href="/journal-cn-9515/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 玻璃钢/复合材料 </a> </span> <span> . 2005</span><span>,第002期</span> </span> </div> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-3500_thesis/02022808890.html">热原子层沉积与等离子体辅助原子层沉积氧化铝薄膜的比较</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yuanxin Zhao&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . Yuanxin Zhao</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=赵元鑫&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,赵元鑫</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Lijun Sang&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,Lijun Sang</a> <span> <a href="/conference-cn-3500/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 2014全国（宁波）防锈润滑包装学术研讨会 </a> <span> <span> . 2014</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020314768913.html">纤维素基复合材料的界面可控润湿性能研究及其在油水分离中的应用</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=王倩&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 王倩</a> <span> . 2018</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/061202692672.html">一种提高发动机热端构件用陶瓷基复合材料力学性能的纤维排布方式</a> <b>[P]</b> . <span> 中国专利： CN106747533B </span> <span> . 2017.12.19</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120109198912.html">一种提高发动机热端构件用陶瓷基复合材料力学性能的纤维排布方式</a> <b>[P]</b> . <span> 中国专利： CN106747533A </span> <span> . 2017-05-31</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130430547931.html">Al<Sub>2</Sub>O<Sub>3 </Sub>atomic layer deposition to enhance the deposition of hydrophobic or hydrophilic coatings on micro-electromechanical devices</a> <b>[P]</b> . <span> 外国专利：  US7553686B2 </span> <span> . 2009-06-30</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：Al <Sub> 2 </ Sub> O <Sub> 3 </ Sub>原子层沉积，以增强疏水或亲水涂层在微机电装置上的沉积 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" 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