Impedance Spectroscopy of Spin‐Cast and Electrochemically Deposited PEDOT:PSS Films on Microfabricated Electrodes with Various Areas

Koutsouras Dimitrios A.; Gkoupidenis Paschalis; Stolz Clemens; Subramanian Vivek; Malliaras George G.; Martin David C.

摘要

Abstract > We have examined the electrochemical impedance spectroscopy (EIS) of PEDOT:PSS‐coated gold electrodes in various electrolytes as a function of temporal frequency (from 0.1 to 10 4 ?Hz) by using a custom‐designed microfabricated substrate. The electrode areas were systematically varied over a broad range in nominal size from 10×10?μm (100?μm 2 ) to 500×500?μm (2.5×10 5 ?μm 2 ). Comparisons were made between spin‐cast PEDOT:PSS crosslinked with GOPS and electrochemically deposited PEDOT:PSS films with similar thicknesses. The impedance spectra of the PEDOT:PSS‐coated electrodes with various sizes could all be reasonably well described by a two‐element equivalent circuit model with a solution resistance R <sub>s</sub> and a film capacitance C . These two parameters together define a characteristic temporal frequency f <sub>c</sub> =1/(2π R <sub>s</sub> C ). By normalizing the impedance with respect to R <sub>s</sub> ( Z <sub>n</sub> =| Z |/ R <sub>s</sub> ) and the frequency with respect to f <sub>c</sub> ( f <sub>n</sub> = f / f <sub>c</sub> ), we found that all of the experimental Bode curves could be collapsed onto a single master plot of Z <sub>n</sub> vs. f <sub>n</sub> . In addition, analytical formulas that allow the estimation of the film impedance magnitude | Z | and phase ? were derived and experimentally validated. These results are of fundamental interest and are also anticipated to be important for the design, characterization, and optimization of conjugated polymer films for interfacing biomedical devices with living tissue. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract XMLNS =“http://www.wiley.com/namespaces/wiley”type =“main”xml：lang =“en”> <标题类型=“main”>抽象</ title> > 我们已经检查了PEDOT的电化学阻抗光谱（EIS）：PSS涂覆的金电极作为时间频率的函数（0.1到10） 4 </ sup> 通过使用定制设计的微制谱基板。在标称尺寸的宽范围内系统地改变电极区域，从10×10？μm（100≤μm 2 </ sup> ）至500×500？μm（2.5×10 5 </ sup> ？μm 2 </ sup> ）。在旋转浇注PCOT之间进行比较：用GOPS交联和电化学沉积的PEDOT：PSS膜，具有相似的厚度。 PEDOT的阻抗光谱：具有各种尺寸的PSS涂覆电极可以通过具有溶液电阻的双元等效电路模型来合理地良好地描述 R </ I> <sub> s </ sub> 和薄膜电容 c </ i> 。这两个参数一起定义了特征时间频率 f </ i> <sub> c </ sub> = 1 /（2π R </ I> <sub> s </ sub> c </ i> ）。通过对抗的阻抗来规范化 R </ I> <sub> s </ sub> （ z </ i> <sub> n </ sub> = | z </ i> | / R </ I> <sub> s </ sub> ）和频率相对于 f </ i> <sub> c </ sub> （ f </ i> <sub> n </ sub> = f </ i> / f </ i> <sub> c </ sub> ），我们发现所有实验弓形曲线都可以折叠到一个主图中 z </ i> <sub> n </ sub> vs. f </ i> <sub> n </ sub> 。另外，允许估计薄膜阻抗幅度的分析公式| z </ i> |和阶段？</ i> 派生和实验验证。这些结果具有基本兴趣，并且还预计对于与活组织接口生物医学装置的共轭聚合物膜的设计，表征和优化是重要的。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-18063/'>《Advanced materials interfaces》</a> <b style="margin: 0 2px;">|</b><span>2017年第9期</span><b style="margin: 0 2px;">|</b><span>共7页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Koutsouras Dimitrios A.&option=202" target="_blank" rel="nofollow">Koutsouras Dimitrios A.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Gkoupidenis Paschalis&option=202" target="_blank" rel="nofollow">Gkoupidenis Paschalis;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Stolz Clemens&option=202" target="_blank" rel="nofollow">Stolz Clemens;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Subramanian Vivek&option=202" target="_blank" rel="nofollow">Subramanian Vivek;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Malliaras George G.&option=202" target="_blank" rel="nofollow">Malliaras George G.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Martin David C.&option=202" target="_blank" rel="nofollow">Martin David C.;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department of BioelectronicsCMP-EMSE MOC880 route de Mimet 13541 Gardanne France;</p> <p>Department of BioelectronicsCMP-EMSE MOC880 route de Mimet 13541 Gardanne France;</p> <p>Department of BioelectronicsCMP-EMSE MOC880 route de Mimet 13541 Gardanne France;</p> <p>Department of Materials Science and EngineeringThe University of DelawareNewark DE 19716 USA;</p> <p>Department of BioelectronicsCMP-EMSE MOC880 route de Mimet 13541 Gardanne France;</p> <p>Department of BioelectronicsCMP-EMSE MOC880 route de Mimet 13541 Gardanne France;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/6960.html" title="特种结构材料">特种结构材料;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=impedance spectroscopy&option=203" rel="nofollow">impedance spectroscopy;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=conjugated polymers&option=203" rel="nofollow">conjugated polymers;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=poly(3&option=203" rel="nofollow">poly(3;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=4-ethylene dioxythiophene) (PEDOT)&option=203" rel="nofollow">4-ethylene dioxythiophene) (PEDOT);</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=organic electronics&option=203" rel="nofollow">organic electronics;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=biomedical electrodes&option=203" rel="nofollow">biomedical electrodes;</a> </p> <div class="translation"> 机译：阻抗光谱;共轭聚合物;聚（3;4-乙烯二氧噻吩）（PEDOT）;有机电子;生物医学电极; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704022434140.html">Impedance Spectroscopy of Spin‐Cast and Electrochemically Deposited PEDOT:PSS Films on Microfabricated Electrodes with Various Areas</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Koutsouras 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H. </a> <span>1986</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：Li / Li sub 3 N电极：电极阻抗谱研究其在有机电解质中的电化学行为</span> </p> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/academic-journal-cn_chemical-journal-chinese-universities_thesis/0201231545977.html">硼掺杂金刚石薄膜电极上二氯酚的电化学阻抗谱研究</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=吕江维&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 吕江维</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=曲有鹏&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,曲有鹏</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=冯玉杰&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,冯玉杰</a> <span> <a href="/journal-cn-10958/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 高等学校化学学报 </a> </span> <span> . 2016</span><span>,第001期</span> </span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/academic-journal-cn_chinese-journal-catalysis_thesis/0201231565408.html">电化学原位表面增强拉曼光谱研究Au@Pd纳米粒子薄膜电极上吸附 CO的斯塔克效应</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=张普&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 张普</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=卫怡&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,卫怡</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=蔡俊&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,蔡俊</a> <span> <a href="/journal-cn-28399/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 催化学报 </a> </span> <span> . 2016</span><span>,第007期</span> </span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/academic-journal-cn_spectroscopy-spectral-analysis_thesis/0201232968776.html">纳米薄膜合金电极上二氧化碳电催化还原的红外光谱研究</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=陈声培&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 陈声培</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=夏盛清&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,夏盛清</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=孙世刚&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,孙世刚</a> <span> <a href="/journal-cn-11127/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 光谱学与光谱分析 </a> </span> <span> . 2000</span><span>,第005期</span> </span> </div> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/academic-journal-cn_acta-physico-chimica-sinica_thesis/0201251108715.html">微圆盘电极上耦合一级均相反应的稳态电流</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=廖川平&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 廖川平</a> <span> <a href="/journal-cn-15102/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 物理化学学报 </a> </span> <span> . 1993</span><span>,第001期</span> </span> </div> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-59666_thesis/020222622710.html">柔性基底上PEDOT∶PSS-C复合薄膜对电极的制备</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=许芳怡&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 许芳怡</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=胡志强&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,胡志强</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=王仁博&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,王仁博</a> <span> <a href="/conference-cn-59666/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 2009全国功能材料科技与产业高层论坛 </a> <span> <span> . 2009</span> </span> </div> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020314905680.html">微流控芯片上薄膜参比电极的制备与应用研究</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=孙雪洁&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 孙雪洁</a> <span> . 2006</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06120113598027.html">一种PEDOT：PSS修饰的碳电极、其制备方法及利用其制得的钙钛矿电池</a> <b>[P]</b> . <span> 中国专利： CN113644208A </span> <span> . 2021-11-12</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/061202754561.html">一种塑基高导电PEDOT:PSS薄膜电极及其制备方法与应用</a> <b>[P]</b> . <span> 中国专利： CN104934540B </span> <span> . 2018.02.06</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130422023572.html">PEDOT/PSS COMPOSITION CAPABLE OF REDUCING SURFACE RESISTANCE OF TRANSPARENT ELECTRODE BY ADDING A WATER-SOLUBLE CONDUCTIVE POLYMER AND A COMPATIBILIZER INTO PEDOT/PSS, AND A PEDOT/PSS FILM USING THE SAME</a> <b>[P]</b> . <span> 外国专利：  KR20120077112A </span> <span> . 2012-07-10</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：通过将水溶性导电聚合物和相容剂添加到PEDOT / PSS中，可以降低透明电极的表面电阻的PEDOT / PSS组合物，以及使用相同的PEDOT / PSS膜 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130411440324.html">PEDOT-PSS PEDOT-PSS Special chemical oxidizing agent for PEDOT-PSS conductive film with excellent oxidation stability and method for patterning conductivity of PEDOT-PSS conductive film using the oxidizing agent</a> <b>[P]</b> . <span> 外国专利：  KR20160116614A </span> <span> . 2016-10-10</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：PEDOT-PSS PEDOT-PSS具有优异的氧化稳定性的PEDOT-PSS导电膜专用化学氧化剂以及使用该氧化剂对PEDOT-PSS导电膜进行构图的方法 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130408776124.html">PEDOT-PSS PEDOT-PSS Special chemical oxidizing agent for PEDOT-PSS conductive film with excellent oxidation stability and method for patterning conductivity of PEDOT-PSS conductive film using the oxidizing agent</a> <b>[P]</b> . <span> 外国专利：  KR101683477B1 </span> <span> . 2016-12-07</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：PEDOT-PSS PEDOT-PSS具有优异的氧化稳定性的PEDOT-PSS导电膜专用化学氧化剂以及使用该氧化剂对PEDOT-PSS导电膜进行构图的方法 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" 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