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首页> 外文期刊>Advanced Powder Technology: The internation Journal of the Society of Powder Technology, Japan >0.5M 0.37Cu 0.13Fe 2O 4 (M?=?Ni, Zn and Mg) ferrite nanoparticle systems]]>
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0.5M 0.37Cu 0.13Fe 2O 4 (M?=?Ni, Zn and Mg) ferrite nanoparticle systems]]>

机译:“:INF>与 0.13 FE 2 O 4 (m?=Δni,zn和mg)铁氧体纳米粒子系统]]]>

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摘要

Ferrite nanoparticles of the composition Co0.5M0.37Cu0.13Fe2O4(M?=?Ni, Zn, and Mg) have been synthesized using sol-gel auto combustion method. Structural properties are investigated using powder X-ray diffraction technique and the results showed a pure spinel crystal structures of the synthesized materials with lattice parameters in the range of 8.3331–8.4793??. Crystallite sizes are calculated using the Scherrer’s formula and the results are found to be in the range of 62.22–82.41?nm. The surface texture and morphological nature of the samples are studied by scanning electron microscopy which depicted clear crystalline nature of the materials. Characteristic vibrational states prevailing in the samples are studied using room temperature Fourier transform infrared spectroscopy. A two-probe DC electrical resistivity measurement of the samples showed a high resistive nature. Room temperature vibrating sample magnetometer measurements revealed the magnetic properties of the samples.
机译:使用溶胶 - 凝胶自燃方法合成了组合物CO 10.5M0.37Cu0.13Fe2O4(M≤N2O,Zn和Mg)的铁氧体纳米粒子。 使用粉末X射线衍射技术研究了结构性性质,结果显示了合成材料的纯尖晶石晶体结构,晶格参数在8.3331-8.4793的范围内。 使用Scherrer的公式计算微晶尺寸,结果被发现在62.22-82.41Ω·nm的范围内。 通过扫描电子显微镜研究样品的表面纹理和形态学性质,其描绘了透明晶体性质的材料。 使用室温傅里叶变换红外光谱研究样品中普遍存在的特征振动状态。 样品的双探针直流电阻率测量显示出高电阻性。 室温振动样品磁力计测量显示样品的磁性。

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