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Vibration-free Stirling cryocooler for high definition microscopy

机译:无振动的斯特林冷冻机,用于高清显微镜

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摘要

The normal operation of high definition Scanning Electronic and Helium Ion microscope tools often relies on maintaining particular components at cryogenic temperatures. This has traditionally been accomplished by using liquid coolants such as liquid Nitrogen. This inherently limits the useful temperature range to above 77 K, produces various operational hazards and typically involves elevated ownership costs, inconvenient logistics and maintenance. Mechanical coolers, over-performing the above traditional method and capable of delivering required (even below 77 K) cooling to the above cooled components, have been well-known elsewhere for many years, but their typical drawbacks, such as high purchasing cost, cooler size, low reliability and high power consumption have so far prevented their wide-spreading. Additional critical drawback is inevitable degradation of imagery performance originated from the wideband vibration export as typical for the operation of the mechanical cooler incorporating numerous movable components. Recent advances in the development of reliable, compact, reasonably priced and dynamically quiet linear cryogenic coolers gave rise to so-called "dry cooling" technologies aimed at eventually replacing the traditional use of outdated liquid Nitrogen cooling facilities. Although much improved these newer cryogenic coolers still produce relatively high vibration export which makes them incompatible with modern high definition microscopy tools. This has motivated further research activity towards developing a vibration free closed-cycle mechanical cryocooler. The authors have successfully adapted the standard low vibration Stirling cryogenic refrigerator (Ricor model K535-LV) delivering 5 W@40 K heat lift for use in vibration-sensitive high definition microscopy. This has been achieved by using passive mechanical counterbalancing of the main portion of the low frequency vibration export in combination with an active feed-forward multi-axes suppression of the residual wideband vibration, thermo-conductive vibration isolation struts and soft vibration mounts. The attainable performance of the resulting vibration free linear Stirling cryocooler (Ricor model K535-ULV) is evaluated through a full-scale experimentation.
机译:高清晰度扫描电子和氦离子显微镜工具的正常运行通常取决于将特定组件保持在低温下。传统上,这是通过使用液态冷却剂(例如液态氮)来实现的。这固有地将有用的温度范围限制在77 K以上,产生各种操作危险,并且通常涉及较高的拥有成本,不便的后勤和维护。机械冷却器性能优于上述传统方法,并且能够向上述冷却的组件提供所需的冷却(甚至低于77 K),多年来在其他地方已广为人知,但它们的典型缺点是,例如高昂的采购成本,冷却器迄今为止,其尺寸,低可靠性和高功耗阻止了它们的广泛普及。另一个严重的缺点是,由于宽带振动输出不可避免地导致图像性能下降,这种宽带振动是结合了许多可移动部件的机械冷却器运行的典型现象。可靠,紧凑,价格合理且动态安静的线性低温冷却器开发的最新进展催生了所谓的“干式冷却”技术,旨在最终取代过时的液氮冷却设备。这些新型的低温冷却器尽管有了很大的改进,但仍然产生了相对较高的振动输出,这使其与现代高清显微镜工具不兼容。这激发了进一步的研究活动,以开发无振动的闭环机械低温冷却器。作者成功地将标准的低振动斯特林低温制冷机(Ricor型号K535-LV)改装成具有5 W @ 40 K的热升力,用于振动敏感的高清显微镜。这是通过对低频振动输出的主要部分进行被动机械平衡以及对剩余宽带振动的主动前馈多轴抑制,热传导隔振支柱和软振动装置的组合来实现的。通过全面的实验评估了所得的无振动线性斯特林低温冷却器(Ricor型号K535-ULV)的可达到的性能。

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