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Comparison of electrocatalytic activity for glucose electrooxidation of gold nanoparticles fabricated by different methods

机译:不同方法制造金纳米颗粒的葡萄糖电氧化电催化活性的比较

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In this study, the gold nanoparticles (AuNPs) without carbon support were prepared using the well-known citrate reduction method. The carbon supported AuNPs nano composites were fabricated by two different approaches: chemical adsorption of AuNPs from the prepared citrate stabilized AuNP colloidal solution on the carbon powder surface and one-pot microwave-assisted synthesis. The nano composites were characterized using scanning electron microscopy (SEM) and inductively coupled plasma optical emission spectroscopy (ICP-OES). The electrocatalytic activity of the prepared catalysts was evaluated for the electrooxidation of glucose in an alkaline media using cyclic voltammetry.
机译:在该研究中,使用众所周知的柠檬酸还原方法制备不含碳载体的金纳米颗粒(AUNP)。 通过两种不同的方法制造碳负载的型纳米复合材料:从制备的柠檬酸盐稳定的碳粉表面上的柠檬酸盐稳定的AUNP胶体溶液和一锅微波辅助合成的化学吸附。 使用扫描电子显微镜(SEM)和电感耦合等离子体光发射光谱(ICP-OES)表征纳米复合材料。 使用循环伏安法评价制备催化剂的电催化活性在碱性介质中的葡萄糖的电氧化。

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