A Facile One‐Step Synthesis of Fe‐Doped g‐C        <sub >3</sub>3        N        <sub >4</sub>4        Nanosheets and Their Improved Visible‐Light Photocatalytic Performance

摘要

Abstract > A simple one‐step pyrolysis process (compared with the routine method of liquid exfoliation and impregnation) was designed to synthesize Fe‐doped graphitic carbon nitride (g‐C <sub>3</sub> N <sub>4</sub> ) nanosheets with NH <sub>4</sub> Cl as dynamic gas template and FeCl <sub>3</sub> as the Fe source. Results of XPS and DRS indicated that the Fe species might exist at the state of Fe 3+ and form Fe?N bonds with N atoms, thereby expanding visible light absorption regions and reducing the band gap of g‐C <sub>3</sub> N <sub>4</sub> nanosheets. Doping certain amounts of Fe could promote the exfoliation and further increase the specific surface area, while excessive Fe might break the sheet structure. The specific surface area of the optimized Fe‐doped g‐C <sub>3</sub> N <sub>4</sub> nanosheets reached 236.52?m 2 ?g ?1 , which was 2.5?times higher than that of g‐C <sub>3</sub> N <sub>4</sub> nanosheets. Among various photocatalysts prepared, the sample (0.5?wt?% FeCl <sub>3</sub> ) exhibited maximum photocatalytic performance in degradation of Methylene Blue and water splitting under visible light irradiation. The degradation rate of MB was about 1.4 and 1.7 times higher than that of pure g‐C <sub>3</sub> N <sub>4</sub> nanosheets and bulk g‐C <sub>3</sub> N <sub>4</sub> , respectively. The H <sub>2</sub> production rate was 536?μmol?h ?1 ?g ?1 , which was 1.8 and 6?times higher than that of pure g‐C <sub>3</sub> N <sub>4</sub> nanosheets and bulk g‐C <sub>3</sub> N <sub>4</sub> , separately. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 设计简单的一步热解过程（与液体去角质和浸渍的常规方法相比）被设计成合成Fe掺杂的石墨碳氮化物（G-C. <sub> 3 </ sub> N. <sub> 4 </ sub> ）纳米片与NH <sub> 4 </ sub> CL作为动态气体模板和FECL <sub> 3 </ sub> 作为FE Source。 XPS和DRS的结果表明FE的FE物种可能存在 3 + </ sup> 与n原子形成Fe键，从而膨胀可见光吸收区域并降低G-C的带隙 <sub> 3 </ sub> N. <sub> 4 </ sub> nanosheets。掺杂一定量的Fe可以促进剥离并进一步增加比表面积，而过量的Fe可能会破坏片状结构。优化的Fe-掺杂G-C的比表面积 <sub> 3 </ sub> N. <sub> 4 </ sub> nanosheets达到236.52？m 2 </ sup> ？G ？1 </ sup> ，比G-C高2.5？ <sub> 3 </ sub> N. <sub> 4 </ sub> nanosheets。在制备的各种光催化剂中，样品（0.5〜wt≤％FECL <sub> 3 </ sub> ）在可见光照射下表现出最大的光催化性能，降解亚甲基蓝色和水分裂。 MB的降解速率比纯G-C高约1.4％， <sub> 3 </ sub> N. <sub> 4 </ sub> Nanosheets和Bulk G-C <sub> 3 </ sub> N. <sub> 4 </ sub> ，分别。 H. <sub> 2 </ sub> 生产率为536？μmol？H. ？1 </ sup> ？G ？1 </ sup> ，这比纯G-C高1.8和6？ <sub> 3 </ sub> N. <sub> 4 </ sub> Nanosheets和Bulk G-C <sub> 3 </ sub> N. <sub> 4 </ sub> ，分别地。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" > 著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-16041/'>《ChemCatChem 》</a> <b style="margin: 0 2px;">|</b><span>2017年第9期</span><b style="margin: 0 2px;">|</b> <span>共8页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li> <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span> <a href="https://www.zhangqiaokeyan.com/clc/1186.html" title="物理化学（理论化学）、化学物理学">物理化学（理论化学）、化学物理学 ;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=g-C 3 N 4 nanosheets&option=203" rel="nofollow">g-C 3 N 4 nanosheets;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=H 2 evolution&option=203" rel="nofollow">H 2 evolution;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=in situ doping&option=203" rel="nofollow">in situ doping;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=iron doping&option=203" rel="nofollow">iron doping;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=photocatalysis&option=203" rel="nofollow">photocatalysis;</a> </p> <div class="translation"> 机译：G-C 3 n 4纳米胸部;H 2演变;原位掺杂;铁掺杂;光催化; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a 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A Facile One‐Step Synthesis of Fe‐Doped g‐C 33 N 44 Nanosheets and Their Improved Visible‐Light Photocatalytic Performance

摘要

A Facile One‐Step Synthesis of Fe‐Doped g‐C ₃3 N ₄4 Nanosheets and Their Improved Visible‐Light Photocatalytic Performance