Connector type‐controlled mesophase structures in poly(propyl ether imine) dendritic liquid crystals of identical dendrimer generations

Kumar Prabhat; Shankar Rao D. S.; Krishna Prasad S.; Jayaraman Narayanaswamy

摘要

ABSTRACT > Poly(propyl ether imine) (PETIM) dendrimers of one to three generations are used as dendritic cores to identify the influence of varying connector types that connect the dendritic core with peripheral mesogens on the emerging liquid crystalline (LC) properties. The LC properties vary in these dendritic liquid crystals, even when the dendrimer generations and thus the number of peripheral mesogenic moieties remain identical. PETIM dendrimer generations one to three, ester and amide connectors varying with succinates, phthalates, and succinamides, are studied herein. Cholesteryl moieties are installed at the peripheries through the above connectors to induce mesogenic properties. These modified dendritic liquid crystals reveal a layered mesophase structure in most ester and amide connector‐derivatives, whereas a third‐generation phthalate ester dendrimer favors a rectangular columnar mesophase structure. A transition from layered to a rectangular columnar structure results by a mere change in the connector varying between a succinate or succinamide or phthalate, within one particular dendrimer generation and without altering the underlying dendrimer core or the number of mesogenic moieties. The study demonstrates that in dendritic liquid crystals with essentially identical chemical constitutions, a change in the connector type connecting the mesogen with the dendrimer core is sufficient to change the mesophase structures. ? 2017 Wiley Periodicals, Inc. J. Polym. Sci., Part A: Polym. Chem. 2017 , 55 , 3665–3678 </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><抽象的xmlns = “http://www.wiley.com/namespaces/wiley” 类型= “主”> <标题类型= “主”>摘要</ TITLE> <P>聚（丙基醚亚胺）（PETIM）一至三个世代的树枝状聚合物被用作芯树突以识别不同的是，树枝状的核与新兴的液晶（LC）性质的周介晶连接的连接器类型的影响。的LC特性在这些树枝状液晶而变化，即使在树枝状聚合物世代，从而外围介晶部分的数目保持相同。 PETIM树枝状聚合物世代一至三个，酯和酰胺连接器与琥珀酸盐，邻苯二甲酸盐，和琥珀变化，在本文中的研究。胆甾醇部分被安装在通过上述连接器的外周以诱导介晶性能。这些修饰的树突状液晶揭示大部分酯和酰胺连接器衍生物的层状中间相结构，而第三代邻苯二甲酸酯树枝状聚合物有利于矩形柱状相结构。过渡从通过在琥珀酸酯或琥珀酰胺或邻苯二甲酸酯之间的连接器变仅仅改变分层，以矩形柱状结构的结果，一个特定代树枝状聚合物内，并且在不改变基本的树枝状聚合物核心或介晶基团的数目。这项研究表明，在具有基本上相同的化学成分的树突状液晶，在连接器类型与树枝状聚合物芯连接所述介晶的变化是否足以改变中间相结构。还是2017 Wiley期刊，Inc.J.Colom。 SCI。，A部分：polym。化学。 <B> 2017 </ B>，<I> 55 </ i>的，3665-3678 </ p> </抽象> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35621/'>《Journal of Polymer Science, Part A. Polymer Chemistry》</a> <b style="margin: 0 2px;">|</b><span>2017年第22期</span><b style="margin: 0 2px;">|</b><span>共14页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Kumar Prabhat&option=202" target="_blank" rel="nofollow">Kumar Prabhat;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Shankar Rao D. S.&option=202" target="_blank" rel="nofollow">Shankar Rao D. S.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Krishna Prasad S.&option=202" target="_blank" rel="nofollow">Krishna Prasad S.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Jayaraman Narayanaswamy&option=202" target="_blank" rel="nofollow">Jayaraman Narayanaswamy;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department of Organic ChemistryIndian Institute of ScienceBangalore 560012 Karnataka India;</p> <p>Centre for Nano and Soft Matter SciencesJalahalli Bangalore 560013 Karnataka India;</p> <p>Centre for Nano and Soft Matter SciencesJalahalli Bangalore 560013 Karnataka India;</p> <p>Department of Organic ChemistryIndian Institute of ScienceBangalore 560012 Karnataka India;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1184.html" title="有机化学">有机化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=dendrimers&option=203" rel="nofollow">dendrimers;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=differential scanning calorimetry (DSC)&option=203" rel="nofollow">differential scanning calorimetry (DSC);</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=glass transition&option=203" rel="nofollow">glass transition;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=liquid crystals&option=203" rel="nofollow">liquid crystals;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=X‐ray&option=203" rel="nofollow">X‐ray;</a> </p> <div class="translation"> 机译：树枝状大分子;差分扫描量热法（DSC）;玻璃过渡;液晶;X射线; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704020726398.html">Connector type‐controlled mesophase structures in poly(propyl ether imine) dendritic liquid crystals of identical dendrimer generations</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Kumar Prabhat&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Kumar Prabhat,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Shankar Rao D. 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