Simultaneously enhanced conductivity and dimensional stability of AAEM by crosslinked polymer microsphere with dense carrier sites

Liu Lei; Sun Guoping

摘要

ABSTRACT > The search for practically applicable alkaline anion exchange membrane (AAEM) has been of continuous interest during the past decades. One of the main obstacles for current AAEM lies in the trade‐off between hydroxide conductivity and dimensional stability. In this contribution, novel quaternary phosphonium polymer microsphere (QPPMS) with crosslinked structure and dense carrier sites is synthesized via precipitation polymerization method, followed by incorporating into chitosan (CS) to prepare composite membrane. Compared with CS, the incorporation of QPPMS endows composite membrane more than two times increased ion exchange capacity (IEC) from 0.39 to 1.2?mmol g ?1 , and highly enhanced water uptake from 90% to 124% with an enhancement of 37.8%. The constructed interfacial and intra‐QPPMS transfer pathways confer almost nine times augment of conductivity at 20°C under 98% relative humidity (RH). Most importantly, the increase of area swelling is limited to 25.0% (from 32% to 40%) due to the crosslinked structure of QPPMS, which is inconceivable for homogeneous membranes and inorganic filler‐based composite membranes. ? 2018 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2018 , 135 , 46715. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><抽象的xmlns = “http://www.wiley.com/namespaces/wiley” 类型= “主”> <标题类型= “主”>摘要</ TITLE> <P>对于实际应用的碱性阴离子交换膜的搜索（AAEM）在过去的几十年中一直持续关注。一个当前AAEM在于氢氧化导电性和尺寸稳定性之间的权衡的主要障碍。在这方面的贡献，新颖季鏻聚合物微球（QPPMS）具有交联结构和密集载体位点是通过沉淀聚合方法，接着掺入壳聚糖（CS），以制备复合膜合成。与CS相比，QPPMS的掺入赋予复合膜的两倍以上从0.39增加的离子交换容量（IEC），以1.2？毫摩尔克<SUP>λ1</ SUP>，和高度增强的水吸收从90％至124％ 37.8％的增强。所构建的界面和帧内QPPMS传递途径赋予下98％的相对湿度（RH）在20电导率几乎九倍扩充℃。最重要的是，面积的增加肿胀限于25.0％（从32％至40％），由于QPPMS的交联结构，这是不可想象的均相膜和无机基填料复合膜。还是2018 Wiley期刊，Inc.J.Phill。聚合物。 SCI。 <B> 2018 </ B>，<I> 135 </ i>的，46715. </ p> </抽象> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" > 著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-33581/'>《Journal of Applied Polymer Science 》</a> <b style="margin: 0 2px;">|</b><span>2018年第40期</span><b style="margin: 0 2px;">|</b> <span>共12页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Liu Lei&option=202" target="_blank" rel="nofollow">Liu Lei;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Sun Guoping&option=202" target="_blank" rel="nofollow">Sun Guoping;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>School of Materials and Chemical EngineeringZhongyuan University of TechnologyZhengzhou 450007 China;</p> <p>School of Materials and Chemical EngineeringZhongyuan University of TechnologyZhengzhou 450007 China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li> <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span> <a href="https://www.zhangqiaokeyan.com/clc/1821.html" title="高分子化合物工业（高聚物工业）">高分子化合物工业（高聚物工业） ;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=batteries and fuel cells&option=203" rel="nofollow">batteries and fuel cells;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=membranes&option=203" rel="nofollow">membranes;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=polyelectrolytes&option=203" rel="nofollow">polyelectrolytes;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=swelling&option=203" rel="nofollow">swelling;</a> </p> <div class="translation"> 机译：电池和燃料电池;膜;聚电解质;肿胀; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704020590038.html">Simultaneously enhanced conductivity and dimensional stability of AAEM by crosslinked polymer microsphere with dense carrier sites</a> <b>[J]</b> . 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