Cascade Annulation of 2-Alkynylthioanisoles with Unsaturated alpha-Bromocarbonyls Leading to Thio-Benzobicyclic Skeletons

Gao Yuzhen; Zhang Pengbo; Li Gang; Zhao Yufen

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Cascade Annulation of 2-Alkynylthioanisoles with Unsaturated alpha-Bromocarbonyls Leading to Thio-Benzobicyclic Skeletons

机译：用不饱和α-溴羰基的2-炔乙基氨基碱的级联环节导致硫代 - 苯甲类环骨架

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摘要

A protocol of Cu-catalyzed annulation of phenylethynylsulfanes with unsaturated alpha-bromocarbonyls for the construction of thio-benzobicyclic skeletons is described. In this single reaction, three new bonds and two new rings can be established, highlighting the step-economics and high efficiency of this protocol.

机译：描述了用不饱和α-溴羰基的苯基乙炔磺酸的Cu催化环催化剂的方案描述于用于构建硫代苯甲酰丙二酰骨架。在这种单一反应中，可以建立三个新的债券和两个新的环，突出了该协议的阶跃经济和高效率。

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《The Journal of Organic Chemistry》 |2018年第22期|共8页
作者
Gao Yuzhen; Zhang Pengbo; Li Gang; Zhao Yufen;
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作者单位

Chinese Acad Sci Fujian Inst Res Struct Matter Key Lab Coal Ethylene Glycol &

Its Related Techno Fuzhou 350002 Fujian Peoples R China;

Xinxiang Med Univ Sch Publ Hlth Xinxiang 453003 Peoples R China;

Chinese Acad Sci Fujian Inst Res Struct Matter Key Lab Coal Ethylene Glycol &

Its Related Techno Fuzhou 350002 Fujian Peoples R China;

Xiamen Univ Coll Chem &

Chem Engn Dept Chem Xiamen 361005 Fujian Peoples R China;

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正文语种 eng
中图分类有机化学;
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1. Cascade Annulation of 2-Alkynylthioanisoles with Unsaturated alpha-Bromocarbonyls Leading to Thio-Benzobicyclic Skeletons [J] . Gao Yuzhen, Zhang Pengbo, Li Gang, The Journal of Organic Chemistry . 2018,第22期

机译：用不饱和α-溴羰基的2-炔乙基氨基碱的级联环节导致硫代 - 苯甲类环骨架
2. Cascade Annulation of 2-Alkynylthioanisoles with Unsaturated alpha-Bromocarbonyls Leading to Thio-Benzobicyclic Skeletons [J] . Gao Yuzhen, Zhang Pengbo, Li Gang, The Journal of Organic Chemistry . 2018,第22期

机译：用不饱和α-溴羰基的2-炔乙基氨基碱的级联环节导致硫代 - 苯甲类环骨架
3. Copper-catalyzed cascade annulation of unsaturated alpha-bromocarbonyls with enynals: a facile access to ketones from aldehydes [J] . Che Chao, Huang Qianwen, Zheng Hanliang, Chemical science . 2016,第7期

机译：铜催化不饱和α-溴代羰基与烯的级联环化：醛类与酮的便捷连接
4. New Triterpene Prosaponin and Sapogenin with Unsaturated Lactone Skeleton From Gynostemma Pentaphfllum and the Antitumor Activities Assay [C] . T.Y.Duan, rnZ.B.Nan, rnL.Y.Xie, Proceedin of 2008 International Conference on Ginseng . 2008

机译：绞股蓝的不饱和内酯骨架的新三萜骨素和皂甙元及其抗肿瘤活性的测定
5. Unsaturated nitriles: Stereoselective annulations and alkylation. [D] . Zhang, Zhiyu. 2004

机译：不饱和腈：立体选择性环和烷基化。
6. Copper-catalyzed cascade annulation of unsaturated α-bromocarbonyls with enynals: a facile access to ketones from aldehydes [O] . Chao Che, Qianwen Huang, Hanliang Zheng, 2016

机译：铜催化不饱和α-溴羰基与烯的级联环化：醛类与酮的便捷连接
7. Cascade Annulation of 2Alkynylthioanisoles with Unsaturated Bromocarbonyls Leading to Thio-Benzobicyclic Skeletons [O] . -1

机译：用不饱和溴羰基的2烷炔酰基氨基甲基纤维素导致硫代苯甲酰基骨烷基骨架

Cascade Annulation of 2-Alkynylthioanisoles with Unsaturated alpha-Bromocarbonyls Leading to Thio-Benzobicyclic Skeletons

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