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首页> 外文期刊>Journal of nanoscience and nanotechnology >Simple Co-Precipitation Synthesis and Characterization Studies of La1-xNixVO3 Perovskites Nanostructures for Humidity Sensing Applications
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Simple Co-Precipitation Synthesis and Characterization Studies of La1-xNixVO3 Perovskites Nanostructures for Humidity Sensing Applications

机译:用于湿度感测应用的La1-xNixVO3钙钛矿纳米结构的简单共沉淀合成和表征研究

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摘要

Ni2+-doped LaVO3 perovskites nanostructures were successfully prepared by a simple coprecipitation method. Powder X-ray diffraction (XRD) pattern confirms that all compositions crystallize with orthorhombic LaVO3 perovskites structure. The lattice parameter decreases with increase in Ni2+ content resulting in the reduction of lattice strain in LaVO3. High resolution scanning electron microscope (HR-SEM) images revealed that the as-prepared samples are crystalline with particle size distribution in 142-250 nm range. The BET studies revealed the surface area of the required samples. The samples were subjected to humidity sensing studies by solid-state electrical conductance studies. The studies revealed that La0.4Ni0.6VO3 is a good candidate for humidity sensors with a higher sensitivity factor (S-f) of 15623.02. The higher S-f of La0.4Ni0.6VO3 is due to the larger surface area of the sample.
机译:通过简单的共沉淀方法成功制备了掺杂Ni2 +的LaVO3钙钛矿纳米结构。粉末X射线衍射(XRD)图案证实所有成分均具有正交晶LaVO3钙钛矿结构结晶。晶格参数随Ni2 +含量的增加而降低,从而导致LaVO3中晶格应变的降低。高分辨率扫描电子显微镜(HR-SEM)图像显示,所制备的样品为晶体,粒度分布在142-250 nm范围内。 BET研究揭示了所需样品的表面积。通过固态电导研究对样品进行湿度感测研究。研究表明,La0.4Ni0.6VO3是湿度传感器的最佳候选者,其灵敏度因子(S-f)为15623.02。 La0.4Ni0.6VO3的S-f较高是由于样品的表面积较大。

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