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Microstructure and microtexture in pure copper processed by high-pressure torsion

机译:高压扭转加工纯铜的组织和微观组织

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The evolution of microstructure and microtexture in high purity copper was examined after processing by high-pressure torsion (HPT). Copper disks were annealed for 1 h at 800 C and later processed monotonously in HPT at ambient temperature for 1/4, 1/2, 1, and 5 turns under a pressure of 6.0 GPa. Electron backscattered diffraction (EBSD) measurements were taken for each disk at three positions: center, mid-radius, and near-edge. Results from EBSD for samples processed between 1/4 and 1 turn indicate the formation of Σ3 twin boundaries by recrystallization before complete microstructural refinement. The results show a gradual increase in the homogeneity of the microstructure with increasing numbers of turns, reaching a stabilized ultrafine-grained structure at 5 turns with a bimodal distribution of fine and coarse grains of 0.15 and 0.5 μm in diameter, respectively. The occurrence of recrystallization in the early straining stages was further supported by examining microtexture development with increasing numbers of turns, where this shows a gradual transition from a shear texture to a mixture of shear and recrystallization and later to a shear texture at high HPT strains. The promotion of recrystallization during HPT is probably related to the high purity of the copper.
机译:通过高压扭转(HPT)处理后,检查了高纯度铜的组织和微观组织的演变。铜盘在800℃退火1小时,然后在HPT中于环境温度下在6.0 GPa的压力下进行1 / 4、1 / 2、1和5圈单调处理。对每个圆盘在三个位置进行了电子背散射衍射(EBSD)测量:中心,中半径和近边缘。 EBSD的结果表明,在1/4和1圈之间加工的样品在完全微观组织细化之前通过重结晶形成了Σ3双晶界。结果显示,随着匝数的增加,微观结构的均匀性逐渐增加,在5匝时达到稳定的超细晶粒结构,分别具有直径为0.15和0.5μm的细晶粒和粗晶粒的双峰分布。通过检查随着匝数增加的微观结构的发展,进一步支持了在早期应变阶段再结晶的发生,其中这表明了从剪切织构到剪切和再结晶的混合物的逐渐过渡,后来又转变为高HPT应变的剪切织构。 HPT过程中重结晶的促进可能与铜的高纯度有关。

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