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Evaluation of EB-PVD deposited Ni-Cr-Al alloy foil

机译:EB-PVD沉积Ni-Cr-Al合金箔的评估

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摘要

Ni-Cr-Al alloy foils were deposited at 900 degrees C from a target of Ni-Cr-Al alloy by EB-PVD, and then annealed at 760 degrees C in a high vacuum furnace for 16 h. Microstructure of as-deposited foil consisted of a large amount of fine grains with mean size of 90 nm. However, after annealing the grains grew obviously to an average size of 4 mu m. In addition, long range chemical ordering of L1(2) type emerged in the annealed specimens, while no evidence of ordering structure were found in the deposited samples. The as-deposited foil exhibited a strong {111} texture on the evaporation side. Twin substructure was dominated within grains of as-deposited and annealed samples. The mechanical properties of the foils were examined using room tensile tests. The ultimate tensile strength of as-deposited and annealed samples is 780 and 767 MPa, respectively. Investigation of fracture surfaces from samples revealed that brittle fracture took place along boundaries of columnar crystals formed on the substrate side, while the equiaxed dimples were dominant on the evaporation side.
机译:Ni-Cr-Al合金箔通过EB-PVD从Ni-Cr-Al合金的靶材在900摄氏度下沉积,然后在高真空炉中于760摄氏度下退火16小时。沉积的箔的微观结构由大量平均尺寸为90 nm的细晶粒组成。但是,退火后,晶粒明显长到平均尺寸为4微米。此外,退火样品中出现了L1(2)型的远距离化学排序,而在沉积的样品中没有发现排序结构的证据。沉积的箔在蒸发侧表现出强的{111}织构。孪晶亚结构在沉积和退火样品的晶粒内占主导地位。使用室内拉伸试验检查箔的机械性能。沉积和退火样品的极限抗拉强度分别为780和767 MPa。对样品的断裂表面进行的研究表明,脆性断裂发生在基板侧形成的柱状晶体的边界,而等轴凹窝在蒸发侧占主导。

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