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Bulk Cu-Cr nanocomposites by high-energy ball milling and spark plasma sintering

机译:高能球磨和放电等离子烧结制备块状Cu-Cr纳米复合材料

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摘要

A set of nanocomposite Cu-Cr powders with the grain size of these immiscible metals below 5 nm were prepared by high-energy ball milling. The powders were then consolidated by short-term (5 min) spark plasma sintering at 700-900 degrees C under pressure (50 MPa) to obtain essentially pore-free pseudo-alloys. The grain sizes in the produced bulk materials remained within the ranges 5-60 nm for Cr-based phase and 200-300 nm for Cu-based matrix. These nanocomposites have a Vickers microhardness up to 3.9 GPa and a specific electrical resistivity in the range 6-9.6 mu Omega cm, which make them promising candidates for the application in high-voltage circuit breakers. (C) 2014 Elsevier B.V. All rights reserved.
机译:通过高能球磨制备了一组纳米复合的Cu-Cr粉末,这些纳米粉末的晶粒尺寸小于5 nm。然后通过在压力(50 MPa)下于700-900摄氏度下短期(5分钟)火花等离子体烧结来固结粉末,从而获得基本上无孔的伪合金。对于Cr基相,所生产的块状材料中的晶粒尺寸保持在5-60nm范围内,而对于Cu基基体,晶粒尺寸保持在200-300nm范围内。这些纳米复合材料具有高达3.9 GPa的维氏显微硬度和6-9.6μOΩcm的比电阻率,这使其成为在高压断路器中应用的有希望的候选者。 (C)2014 Elsevier B.V.保留所有权利。

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