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Preparation of Ni/MgOZrO2 nanocrystals by citrate sol-gel method

机译:柠檬酸溶胶-凝胶法制备Ni / MgOZrO2纳米晶

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摘要

Ni/MgOZrO_2 nanocrystals were prepared by the citrate sol-gel method and characterized by X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, scanning electron microscopy (SEM) and nitrogen adsorption methods. Results show that the powders prepared by calcination for 4 h at a temperature of 800 deg C have a particle size of 15 nm and possess a surface area of 145 m~2/g.
机译:采用柠檬酸盐溶胶-凝胶法制备了Ni / MgOZrO_2纳米晶体,并通过X射线衍射(XRD),傅立叶变换红外光谱(FTIR),扫描电子显微镜(SEM)和氮吸附法对其进行了表征。结果表明,在800℃下煅烧4h制得的粉末的粒径为15nm,表面积为145m 2 / g。

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