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Determination of Bisphenol A in Canned Foods by Immunoaffinity Chromatography,HPLC,and Fluorescence Detection

机译:免疫亲和色谱,HPLC和荧光检测法测定罐头食品中的双酚A

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摘要

Bisphenol A(BPA)concentrations were determined in canned beverages,fruits,vegetables,and fat-containing foodstuffs bought in Austrian supermarkets.The analysis method consisted of sol-gel immunoaffinity Chromatography followed by high-performance liquid Chromatography with fluorescence detection.With one exception traces of BPA were detected in all samples.BPA recovery strongly depended on the food matrix,ranging from 27% in goulash to 103% in a lemon soft drink.The results obtained allow a more realistic picture of the BPA exposure caused by cans with an epoxy resin protective coating because-in contrast to several previous studies-only those fractions of the can contents that are actually consumed were analyzed.BPA concentrations ranging from 0.1 ng/mL(lemon soft drink)to 38 ng/g(ready-to eat soup from Thailand)were significantly lower than the European Union migration limit of 0.6 mg of BPA/kg of food.
机译:在奥地利超市购买的罐装饮料,水果,蔬菜和含脂肪食品中测定双酚A(BPA)浓度。分析方法包括溶胶-凝胶免疫亲和色谱法,高效液相色谱法和荧光检测法。所有样品中都检测到痕量的BPA.BPA的回收率在很大程度上取决于食物的基质,从炖牛肉中的27%到柠檬软饮料中的103%不等。环氧树脂保护涂料,因为与先前的研究不同,仅分析了罐头中实际消耗的那些部分。双酚A浓度范围从0.1 ng / mL(柠檬汽水)到38 ng / g(即食食品)来自泰国的汤)远远低于欧盟规定的每公斤食物0.6 mg BPA的迁移极限。

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