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Fabrication and properties of thermal sprayed stainless steel-based nanocomposite coatings

机译:热喷涂不锈钢基纳米复合涂层的制备和性能

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Stainless steel-based feedstock powders with nano-iron oxide particles (from direct addition and thermal oxidation) were prepared by ball milling and oxidation process, respectively. It was found that iron oxide nanoparticles were on the surface of stainless steel powders in the form of particulates (deliberate addition of magnetite and hematite) or nanoplatelets (thermal oxidation). The powders were thermal sprayed by low velocity oxy-fuel (LVOF) technique. The stainless steel-based coatings had the typical thermal spray microstructure, including splats, oxide layers, unmelted particles and pores. There were no nanoparticles seen in the microstructure due to complete oxide melting at the flame spray temperature and iron oxide in all coatings was in the form of hematite. Considering physical properties, porosity was decreased when there were second phase nanoparticles and thickness was very similar except the coating with hematite addition. Hardness of the coatings was slightly increased when incorporating with iron oxide nanoparticles. Sliding wear rate and friction coefficient of the nanocomposite coatings were lower than that of the pure stainless steel. Iron oxide nanoparticles could improve hardness and sliding wear resistance in the stainless steel-based coatings due to an increasing amount of iron oxide in the coatings. (C) 2015 Elsevier B.V. All rights reserved.
机译:通过球磨和氧化工艺分别制备了具有纳米氧化铁颗粒(直接添加和热氧化)的不锈钢基原料粉末。已发现,氧化铁纳米颗粒以颗粒(故意添加磁铁矿和赤铁矿)或纳米片(热氧化)的形式存在于不锈钢粉末表面。通过低速含氧燃料(LVOF)技术对粉末进行热喷涂。不锈钢基涂层具有典型的热喷涂微观结构,包括喷溅,氧化层,未熔化的颗粒和孔。由于在火焰喷射温度下氧化物完全熔化,因此在微观结构中没有看到纳米颗粒,并且所有涂层中的氧化铁均为赤铁矿形式。考虑到物理性质,当存在第二相纳米颗粒时,孔隙率降低,并且厚度与添加了赤铁矿的涂层非常相似。当与氧化铁纳米粒子结合时,涂层的硬度略有增加。纳米复合涂层的滑动磨损率和摩擦系数低于纯不锈钢。由于涂层中氧化铁的量增加,氧化铁纳米颗粒可以提高不锈钢基涂层的硬度和抗滑动磨损性。 (C)2015 Elsevier B.V.保留所有权利。

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