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Fatigue strength of diamond coatings' interface assessed by inclined impact test

机译:通过倾斜冲击试验评估金刚石涂层界面的疲劳强度

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The inclined impact test is an efficientmethod for characterizing the fatigue strength of interfaces of nanocrystalline diamond coatings (NCD). During this test, an oscillating oblique load induces repetitive shear stresses into the region between film and its substrate. Inclined impact tests were conducted on NCD coated specimens with a thickness of ca. 5 μmat forces up to 850 N and 1.5 million loading cycles. The related imprints were evaluated by confocal microscopy measurements and EDX micro-analyses. Dependent on the applied load, after a certain number of impacts, damages in the film interface region develop resulting in coating detachment. In thisway, residual stresses of the film are released leading to its lifting (bulge formation). The bulges are destroyed by further repetitive impacts and the coating is totally removed. The geometry of the developed NCD coating's bulges can be effectively described by appropriate Finite Element Method (FEM) supported calculations. Based on the attained impact test results, Woehler-like diagrams were developed for monitoring the fatigue failure or endurance of NCD coatings at various impact conditions. Employing such diagrams, the fatigue strength of NCD coatings can be assessed. According to the attainedWoehler-like diagrams, a threshold load of 730 N exists for the film delamination by fatigue in the investigated case.
机译:倾斜冲击试验是表征纳米晶金刚石涂层(NCD)界面疲劳强度的有效方法。在此测试过程中,摆动的斜向载荷会在薄膜与其基材之间的区域中产生重复的剪切应力。倾斜冲击试验是在NCD涂层的样品上进行的,厚度为。 5μmat的作用力高达850 N,并具有150万次加载循环。通过共聚焦显微镜测量和EDX显微分析评估相关的印记。取决于所施加的载荷,在一定数量的冲击之后,在膜界面区域中出现损坏,从而导致涂层脱离。这样,薄膜的残余应力得以释放,从而导致薄膜抬起(凸出)。凸起被进一步的重复冲击破坏,并且涂层被完全去除。可以通过适当的有限元方法(FEM)支持的计算有效地描述已开发的NCD涂层凸起的几何形状。根据获得的冲击测试结果,开发了类似Woehler的图表,用于监测NCD涂层在各种冲击条件下的疲劳失效或耐久性。使用此类图表,可以评估NCD涂层的疲劳强度。根据所获得的类似Woehler的图,在所研究的情况下,存在730 N的阈值载荷,用于疲劳引起的膜分层。

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