Divergent synthesis of (6S,1 ' S,2 ' R)-hydroxypestalotin via tandem conjugate addition-lactonization sequence

Mallula Venkata Satyanarayana; Srinivas Batthula; Krishna Palakodety Radha

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Divergent synthesis of (6S,1 ' S,2 ' R)-hydroxypestalotin via tandem conjugate addition-lactonization sequence

机译：通过串联共轭加成-内酯化序列（6S，1'S，2'R）-羟基甜菜碱的不同合成

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摘要

The stereoselective synthesis of (65,1'S,2'R)-hydroxypestalotin from trans-hex-2-en-1-ol utilizing asymmetric dihydroxylation and Luche's reduction and tandem conjugative addition-lactonization as the key steps is reported. (C) 2015 Elsevier Ltd. All rights reserved.

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《Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry 》 |2015年第9期| 共3页
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Mallula Venkata Satyanarayana; Srinivas Batthula; Krishna Palakodety Radha;
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正文语种 eng
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关键词
Hydroxypestalotin (LL-P880 beta); Jacobsen's hydrolytic kinetic resolution; Luche's reduction; Conjugative addition-lactonization;

机译：羟佩斯塔洛汀（LL-P880 beta）;雅各布森的水解动力学拆分;卢氏还原;共轭加内酯化;

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1. Divergent synthesis of (6S,1 ' S,2 ' R)-hydroxypestalotin via tandem conjugate addition-lactonization sequence [J] . Mallula Venkata Satyanarayana, Srinivas Batthula, Krishna Palakodety Radha Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2015 ,第9期

机译：通过串联共轭加成-内酯化序列（6S，1'S，2'R）-羟基甜菜碱的不同合成
2. Divergent synthesis of L-685,458 and its analogues involving one-pot intramolecular tandem sequence reaction [J] . Si Chang-Mei, Mao Zhuo-Ya, Zhou Zhu, Tetrahedron . 2015 ,第50期

机译：一锅内分子串联反应的L-685,458及其类似物的不同合成
3. A concise enantioselective synthesis and cytotoxic evaluation of the anticancer rotenoid deguelin enabled by a tandem Knoevenagel/conjugate addition/ decarboxylation sequence [J] . Rebecca L. Farmer, Karl A. Scheidt Chemical science . 2013 ,第8期

机译：串联Knoevenagel /缀合物添加/脱羧序列可实现抗癌类胡萝卜素deguelin的简明对映选择性合成和细胞毒性评估
4. New straightforward synthesis of non-conjugated ynones by ozonolysis -oxo-elimination reaction sequence [C] . Andrey E. Shesheney, Ekaferina V. Boltukhina, Ilya M. Lyapkalo European Symposium on Organic Chemistry . 2009

机译：通过臭氧溶解 - 过氧 - 消除反应序列的新直接合成非共轭氧化钇
5. I. Studies toward the synthesis of cephalotaxine. II. Tandem Claisen rearrangement of ynediols. III. Synthesis of substrates to study the stereochemistry of the conjugate 1,4-elimination reaction [D] . Baevsky, Matthew Frank 1991

机译：I.关于头孢他辛合成的研究。二。炔二醇的串联克莱森重排。三，合成底物以研究共轭1,4-消除反应的立体化学
6. A Concise Enantioselective Synthesis and Cytotoxic Evaluation of the Anticancer Rotenoid Deguelin Enabled by a Tandem Knoevenagel/Conjugate Addition/Decarboxylation Sequence [O] . Rebecca L. Farmer, Karl A. Scheidt -1

机译：串联Knoevenagel /缀合物加成/脱羧序列的抗癌类胡萝卜素Deguelin的简明对映选择性合成和细胞毒性评价。
7. Comparison of conserved structural and regulatory domains within divergent 16S rRNA–23S rRNA spacer sequences of cyanobacteria The GenBank accession numbers for the sequences reported in this paper are AF180968 and AF180969 for ITS-L and ITS-S, respectively. [O] . Isabelle Iteman, Rosmarie Rippka, Nicole Tandeau de Marsac, 2000

机译：分发16S rRNA-23s rRNA-23s rRNA-23s rRNA间隔序列的节省结构和调节域的比较分别是本文报告的序列的GenBank登录号分别为其-L及其-S的AF180968和AF180969。
8. Synthesis of Conjugated Polymers with Alternating Aromatic and Quinonoid Sequences Via Elimination on Precursors [R] . Jenekhe, S. A. 1986

机译：通过前体消除合成具有交替芳香和醌类序列的共轭聚合物

Divergent synthesis of (6S,1 ' S,2 ' R)-hydroxypestalotin via tandem conjugate addition-lactonization sequence

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