Deuterodehalogenation—a mild method for synthesising deuterated heterocycles

Craig S. Donald; Thomas A. Moss; Gary M. Noonan

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Deuterodehalogenation—a mild method for synthesising deuterated heterocycles

机译：氘代卤代化-一种合成氘代杂环的温和方法

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摘要

We report a mild and efficient method for introducing deuterium into a range of heterocycles by reacting readily available halide analogues in a deuterodehalogenation reaction using D8-IPA or Et3SiD under palladium-catalysed conditions.

机译：我们报告了一种温和而有效的方法，可通过使用D8-IPA或Et3SiD在钯催化的条件下，在氘代卤代反应中将随时可用的卤化物类似物反应，将氘引入一系列杂环中。

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《Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry》 |2014年第22期|共3页
作者
Craig S. Donald; Thomas A. Moss; Gary M. Noonan;
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正文语种 eng
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关键词
Deuterium; Deuterodehalogenation; Heterocycles; Metabolism;

机译：氘;氘代脱卤;杂环;代谢;

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1. Deuterodehalogenation—a mild method for synthesising deuterated heterocycles [J] . Craig S. Donald, Thomas A. Moss, Gary M. Noonan Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2014,第22期

机译：氘代卤代化-一种合成氘代杂环的温和方法
2. In situ generated stabilized phosphorus ylides mediated a mild and efficient method for the preparation of some new sterically congested electron-poor N-vinylated heterocycles [J] . Bahrami Mehdi, Ramazani Ali, Hanifehpour Younes, Phosphorus, Sulfur, and Silicon and the Related Elements . 2016,第10a12期

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3. In situ generated stabilized phosphorus ylides mediated a mild and efficient method for the preparation of some new sterically congested electron-poor N-vinylated heterocycles [J] . Bahrami Mehdi, Ramazani Ali, Hanifehpour Younes, Phosphorus, Sulfur, and Silicon and the Related Elements . 2016,第10a12期

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4. Synthesis of benzofused six-membered heterocycles: Rinsing the methods in the river of sustainability [C] . Stefano Menichetti School "A. Corbella" . 2012

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5. Transforming shape: A simultaneous approach to the body, cloth and print for textile and garment design (synthesising CAD with manual methods) [D] . Townsend, Katherine. 2003

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6. Mild Conditions for Deuteration of Primary and Secondary Arylamines for the Synthesis of Deuterated Optoelectronic Organic Molecules [O] . Anwen M. Krause-Heuer, Nageshwar R. Yepuri, Tamim A. Darwish, 2014

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7. Mild conditions for Deuteration of primary and secondary Arylamines for the synthesis of deuterated optoelectronic organic molecules [O] . Krause-Heuer, AM, Yepuri, NR, Darwish, TA, 2016

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8. Results from a Prenatal Oral Developmental Toxicity Study in Rats with Nitrogen containing Heterocycle, Substituted (Substance A) (Star 2), Nitrogen containing Heterocycle, Substituted (Substance B) (Star 2), Nitrogen containing Heterocycle, Substituted (Substance C) (Star 2), Nitrogen containing Heterocycle, Substituted (Substance D) (Star 2) Nitrogen containing Heterocycle, Substituted (Substance E) (Star 2). [R] . 2009

机译：含氮杂环，取代（物质a）（星2），含氮杂环，取代（物质B）（星2），含氮杂环，取代（物质C）（星）的大鼠的产前口腔发育毒性研究结果2），含氮杂环，取代（物质D）（星形2）含氮杂环，取代（物质E）（星形2）。

Deuterodehalogenation—a mild method for synthesising deuterated heterocycles

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